Determination of low levels of uranium in solutions obtained by acid attack on phosphate rock

The uranium present in the leach liquors obtained by attack on phosphate rock with sulphuric acid can be extracted with di(2-ethylhexyl)phosphoric acid and TBP after oxidation of any iron(II), and then stripped at 65° with iron(II) in 8.6 M phosphoric acid. The uranium is finally determined with ars...

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Veröffentlicht in:Talanta (Oxford) 1977-02, Vol.24 (2), p.117-120
1. Verfasser: Bunus, Florin T.
Format: Artikel
Sprache:eng
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Zusammenfassung:The uranium present in the leach liquors obtained by attack on phosphate rock with sulphuric acid can be extracted with di(2-ethylhexyl)phosphoric acid and TBP after oxidation of any iron(II), and then stripped at 65° with iron(II) in 8.6 M phosphoric acid. The uranium is finally determined with arsenazo III.
ISSN:0039-9140
1873-3573
DOI:10.1016/0039-9140(77)80159-8