Atmospheric Pressure Scanning Transmission Electron Microscopy

Scanning transmission electron microscope (STEM) images of gold nanoparticles at atmospheric pressure have been recorded through a 0.36 mm thick mixture of CO, O2, and He. This was accomplished using a reaction cell consisting of two electron-transparent silicon nitride membranes. Gold nanoparticles...

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Veröffentlicht in:Nano Letters 2010-03, Vol.10 (3), p.1028-1031
Hauptverfasser: de Jonge, Niels, Bigelow, Wilbur C, Veith, Gabriel M
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Bigelow, Wilbur C
Veith, Gabriel M
description Scanning transmission electron microscope (STEM) images of gold nanoparticles at atmospheric pressure have been recorded through a 0.36 mm thick mixture of CO, O2, and He. This was accomplished using a reaction cell consisting of two electron-transparent silicon nitride membranes. Gold nanoparticles of a full width at half-maximum diameter of 1.0 nm were visible above the background noise, and the achieved edge resolution was 0.4 nm in accordance with calculations of the beam broadening.
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subjects ATMOSPHERIC PRESSURE
Computer Simulation
Cross-disciplinary physics: materials science
rheology
DESIGN
ELECTRON MICROSCOPES
Exact sciences and technology
GOLD
Gold - chemistry
INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY
Materials science
Microscopy, Electron, Scanning Transmission - methods
Models, Chemical
Nanocrystalline materials
Nanoparticles - chemistry
Nanoparticles - ultrastructure
Nanoscale materials and structures: fabrication and characterization
Physics
RESOLUTION
SAMPLE HOLDERS
SCANNING ELECTRON MICROSCOPY
TRANSMISSION ELECTRON MICROSCOPY
title Atmospheric Pressure Scanning Transmission Electron Microscopy
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