X-ray structure of the (2,2,6,6-tetramethylpiperidin-1-oxyl-4-yl)2,3,4,6- tetra-O-acetyl-beta-D-glucopyranoside
The crystal structure of (2,2,6,6-tetramethylpiperidin-1-oxyl-4-yl)2,3,4,6-tetra-O-acetyl-b eta-D- glucopyranoside, C23H36NO11, is orthorhombic, P2(1)2(1)2(1), with Z4, a 6.207(1), b 14.219(1), and c 30.986(2) A. It was solved by use of the MULTAN program and refined to a RW value 0.044, for 2874 ob...
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| Veröffentlicht in: | Carbohydrate research 1991-09, Vol.218, p.1-8 |
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| container_title | Carbohydrate research |
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| creator | Cinget, F Gagnaire, D Grand, A Vottero, P J |
| description | The crystal structure of (2,2,6,6-tetramethylpiperidin-1-oxyl-4-yl)2,3,4,6-tetra-O-acetyl-b eta-D- glucopyranoside, C23H36NO11, is orthorhombic, P2(1)2(1)2(1), with Z4, a 6.207(1), b 14.219(1), and c 30.986(2) A. It was solved by use of the MULTAN program and refined to a RW value 0.044, for 2874 observed reflections. It has a head to tail arrangement, each piperidine heterocycle being located between the carbohydrate residues of each neighboring molecule. |
| doi_str_mv | 10.1016/0008-6215(91)84081-O |
| format | Article |
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It was solved by use of the MULTAN program and refined to a RW value 0.044, for 2874 observed reflections. 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It was solved by use of the MULTAN program and refined to a RW value 0.044, for 2874 observed reflections. 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It was solved by use of the MULTAN program and refined to a RW value 0.044, for 2874 observed reflections. It has a head to tail arrangement, each piperidine heterocycle being located between the carbohydrate residues of each neighboring molecule.</abstract><cop>Netherlands</cop><pmid>1802381</pmid><doi>10.1016/0008-6215(91)84081-O</doi><tpages>8</tpages></addata></record> |
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| source | MEDLINE; ScienceDirect Journals (5 years ago - present) |
| subjects | Crystallography Cyclic N-Oxides - chemistry Glucose - analogs & derivatives Glucose - chemistry Models, Molecular Spin Labels |
| title | X-ray structure of the (2,2,6,6-tetramethylpiperidin-1-oxyl-4-yl)2,3,4,6- tetra-O-acetyl-beta-D-glucopyranoside |
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