X-ray structure of the (2,2,6,6-tetramethylpiperidin-1-oxyl-4-yl)2,3,4,6- tetra-O-acetyl-beta-D-glucopyranoside

X-ray structure of the (2,2,6,6-tetramethylpiperidin-1-oxyl-4-yl)2,3,4,6- tetra-O-acetyl-beta-D-glucopyranoside

The crystal structure of (2,2,6,6-tetramethylpiperidin-1-oxyl-4-yl)2,3,4,6-tetra-O-acetyl-b eta-D- glucopyranoside, C23H36NO11, is orthorhombic, P2(1)2(1)2(1), with Z4, a 6.207(1), b 14.219(1), and c 30.986(2) A. It was solved by use of the MULTAN program and refined to a RW value 0.044, for 2874 ob...

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Veröffentlicht in:Carbohydrate research 1991-09, Vol.218, p.1-8
Hauptverfasser: Cinget, F, Gagnaire, D, Grand, A, Vottero, P J
Format: Artikel
Sprache:eng
Schlagworte:
Crystallography
Cyclic N-Oxides - chemistry
Glucose - analogs & derivatives
Glucose - chemistry
Models, Molecular
Spin Labels
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Zusammenfassung:The crystal structure of (2,2,6,6-tetramethylpiperidin-1-oxyl-4-yl)2,3,4,6-tetra-O-acetyl-b eta-D- glucopyranoside, C23H36NO11, is orthorhombic, P2(1)2(1)2(1), with Z4, a 6.207(1), b 14.219(1), and c 30.986(2) A. It was solved by use of the MULTAN program and refined to a RW value 0.044, for 2874 observed reflections. It has a head to tail arrangement, each piperidine heterocycle being located between the carbohydrate residues of each neighboring molecule.
ISSN:0008-6215
DOI:10.1016/0008-6215(91)84081-O