Structural Analysis of Partially Acetylated Glycosides by Refocused-Decoupled Insensitive Nuclei Enhanced by Polarization Transfer (INEPT) Experiments: A Qualitative and Quantitative Method

The application of the refocused-decoupled INEPT pulse sequence in 13C-NMR spectroscopy allows, in conjonction with computer simulations, a straightforward editing of the spectra of a raw mixture of glycosidic compounds.

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Bibliographische Detailangaben
Veröffentlicht in:	Chemical & pharmaceutical bulletin 2002, Vol.50(8), pp.1114-1117
Hauptverfasser:	Pouységu, Laurent, Jéso, Bernard De, Lartigue, Jean-Claude, Pétraud, Michel, Ratier, Max
Format:	Artikel
Sprache:	eng
Schlagworte:	13C-NMR acetylated glycosides Acetylation Atomic and molecular physics Bioconversions. Hemisynthesis Biological and medical sciences Biotechnology carbohydrate chemistry computer simulations enzymatic hydrolysis Exact sciences and technology Fundamental and applied biological sciences. Psychology Glycosides - analysis Glycosides - chemistry Methods. Procedures. Technologies Molecular properties and interactions with photons Molecular Structure Nuclear Magnetic Resonance, Biomolecular - methods Nuclear resonance and relaxation Physics refocused-decoupled INEPT
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Beschreibung
Zusammenfassung:	The application of the refocused-decoupled INEPT pulse sequence in 13C-NMR spectroscopy allows, in conjonction with computer simulations, a straightforward editing of the spectra of a raw mixture of glycosidic compounds.
ISSN:	0009-2363 1347-5223
DOI:	10.1248/cpb.50.1114