Relative and Absolute Stereochemistry of the Didemnaketals, Metabolites of a Palauan Ascidian, Didemnum sp

The absolute stereochemistry of the heptaprenoids didemnaketals B (2) and C (3), isolated from a Palauan ascidian, was determined using a combination of degradation and derivatization experiments, chiral shift methods, and comparison of fragments to known compounds.

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Bibliographische Detailangaben
Veröffentlicht in:	Organic letters 2002-05, Vol.4 (10), p.1699-1702
Hauptverfasser:	Salomon, Christine E, Williams, David H, Lobkovsky, Emil, Clardy, Jon C, Faulkner, D. John
Format:	Artikel
Sprache:	eng
Schlagworte:	Animals Anti-HIV Agents - chemistry Anti-HIV Agents - isolation & purification Anti-HIV Agents - pharmacology Crystallography, X-Ray Esters - chemistry Esters - isolation & purification Esters - pharmacology HIV-1 - drug effects Indicators and Reagents Magnetic Resonance Spectroscopy Models, Molecular Molecular Conformation Oxidation-Reduction Spiro Compounds - chemistry Spiro Compounds - isolation & purification Spiro Compounds - pharmacology Urochordata - chemistry
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Beschreibung
Zusammenfassung:	The absolute stereochemistry of the heptaprenoids didemnaketals B (2) and C (3), isolated from a Palauan ascidian, was determined using a combination of degradation and derivatization experiments, chiral shift methods, and comparison of fragments to known compounds.
ISSN:	1523-7060 1523-7052
DOI:	10.1021/ol025904z