A clamp-type pressure cell for high energy x-ray diffraction

We present a clamp-type pressure cell for high energy x-ray diffraction. The pressure cell was specifically designed for studies of weak superstructure reflections at low temperatures in transition metal oxides, resulting from, e.g., charge density modulations. Using a photon energy of E = 100 keV ,...

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Veröffentlicht in:Review of scientific instruments 2008-03, Vol.79 (3), p.033906-033906-6
Hauptverfasser: Zimmermann, M. v., Nowak, R., Gu, G. D., Mennerich, C., Klauss, H.-H., Hücker, M.
Format: Artikel
Sprache:eng
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Zusammenfassung:We present a clamp-type pressure cell for high energy x-ray diffraction. The pressure cell was specifically designed for studies of weak superstructure reflections at low temperatures in transition metal oxides, resulting from, e.g., charge density modulations. Using a photon energy of E = 100 keV , the bulk properties of single crystals with a volume of typically 2 - 5 mm 3 can be studied in transmission geometry. To demonstrate the performance of the pressure cell, we present data on the charge stripe order in the high-temperature superconductor La 1.875 Ba 0.125 Cu O 4 .
ISSN:0034-6748
1089-7623
DOI:10.1063/1.2889162