A clamp-type pressure cell for high energy x-ray diffraction
We present a clamp-type pressure cell for high energy x-ray diffraction. The pressure cell was specifically designed for studies of weak superstructure reflections at low temperatures in transition metal oxides, resulting from, e.g., charge density modulations. Using a photon energy of E = 100 keV ,...
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Veröffentlicht in: | Review of scientific instruments 2008-03, Vol.79 (3), p.033906-033906-6 |
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Hauptverfasser: | , , , , , |
Format: | Artikel |
Sprache: | eng |
Online-Zugang: | Volltext |
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Zusammenfassung: | We present a clamp-type pressure cell for high energy x-ray diffraction. The pressure cell was specifically designed for studies of weak superstructure reflections at low temperatures in transition metal oxides, resulting from, e.g., charge density modulations. Using a photon energy of
E
=
100
keV
, the bulk properties of single crystals with a volume of typically
2
-
5
mm
3
can be studied in transmission geometry. To demonstrate the performance of the pressure cell, we present data on the charge stripe order in the high-temperature superconductor
La
1.875
Ba
0.125
Cu
O
4
. |
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ISSN: | 0034-6748 1089-7623 |
DOI: | 10.1063/1.2889162 |