Effects of sample preparation conditions on biomolecular solid-state NMR lineshapes

Sample preparation conditions with the 46 kDa enzyme complex of 5-enolpyruvyl-shikimate-3-phosphate (EPSP) synthase, shikimate-3-phosphate (S3P) and glyphosate (GLP) have been examined in an attempt to reduce linewidths in solid-state NMR spectra. The linewidths of 31P resonances associated with enz...

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Veröffentlicht in:Journal of biomolecular NMR 1998-10, Vol.12 (3), p.417-421
Hauptverfasser: Jakeman, D L, Mitchell, D J, Shuttleworth, W A, Evans, J N
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Sprache:eng
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