Azide monoliths as convenient flow reactors for efficient Curtius rearrangement reactions

The preparation and use of an azide-containing monolithic reactor is described for use in a flow chemistry device and in particular for conducting Curtius rearrangement reactions via acid chloride inputs.

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Bibliographische Detailangaben
Veröffentlicht in:	Organic & biomolecular chemistry 2008-01, Vol.6 (9), p.1587-1593
Hauptverfasser:	Baumann, Marcus, Baxendale, Ian R, Ley, Steven V, Nikbin, Nikzad, Smith, Christopher D
Format:	Artikel
Sprache:	eng
Schlagworte:	Azides - chemistry Carbamates - chemical synthesis Carbamates - chemistry Chromatography, High Pressure Liquid - instrumentation Chromatography, High Pressure Liquid - methods Equipment Design Ion Exchange Resins - chemistry Mass Spectrometry - instrumentation Mass Spectrometry - methods Molecular Structure Particle Size Porosity Quaternary Ammonium Compounds - chemistry Sensitivity and Specificity Surface Properties Urea - analogs & derivatives Urea - chemical synthesis Urea - chemistry
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Beschreibung
Zusammenfassung:	The preparation and use of an azide-containing monolithic reactor is described for use in a flow chemistry device and in particular for conducting Curtius rearrangement reactions via acid chloride inputs.
ISSN:	1477-0520 1477-0539
DOI:	10.1039/b801634h