Analysis of trimethyl carboxyphosphate by gas chromatography–mass spectrometry

Analysis of trimethyl carboxyphosphate samples by gas chromatography–mass spectrometry, using typical conditions resulted in significant decomposition of the analyte. Optimization of injection conditions, including conditioning of the injection port liner, produced a dramatic increase in observed pe...

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Veröffentlicht in:	Analytical biochemistry 2008-05, Vol.376 (2), p.283-285
Hauptverfasser:	McIldowie, Matthew J., Attwood, Paul V., Reeder, Anthony, Piggott, Matthew J.
Format:	Artikel
Sprache:	eng
Schlagworte:	Anhydrides - analysis Anhydrides - chemistry Gas Chromatography-Mass Spectrometry - methods Molecular Structure Organophosphates - analysis Organophosphates - chemistry Phosphates - analysis Phosphates - chemistry Reproducibility of Results
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Beschreibung
Zusammenfassung:	Analysis of trimethyl carboxyphosphate samples by gas chromatography–mass spectrometry, using typical conditions resulted in significant decomposition of the analyte. Optimization of injection conditions, including conditioning of the injection port liner, produced a dramatic increase in observed peak areas and afforded an effective method for detection of trimethyl carboxyphosphate at the
ISSN:	0003-2697 1096-0309
DOI:	10.1016/j.ab.2008.01.027