Step-by-Step Route for the Synthesis of Metal−Organic Frameworks

Step-by-Step Route for the Synthesis of Metal−Organic Frameworks

Using a novel layer-by-layer approach we have deposited metal−organic open frameworks (MOFs) based on benzenetricarboxylic acid ligands and Cu(II)-ions on a COOH-terminated organic surface. The deposited layers were characterized using a number of surface analysis techniques. XRD measurements show t...

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Veröffentlicht in:Journal of the American Chemical Society 2007-12, Vol.129 (49), p.15118-15119
Hauptverfasser: Shekhah, Osama, Wang, Hui, Kowarik, Stefan, Schreiber, Frank, Paulus, Michael, Tolan, Metin, Sternemann, Christian, Evers, Florian, Zacher, Denise, Fischer, Roland A, Wöll, Christof
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Sprache:eng
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Zusammenfassung:Using a novel layer-by-layer approach we have deposited metal−organic open frameworks (MOFs) based on benzenetricarboxylic acid ligands and Cu(II)-ions on a COOH-terminated organic surface. The deposited layers were characterized using a number of surface analysis techniques. XRD measurements show that the MOFs deposited using this method have the same bulk structure of HKUST-1.
ISSN:0002-7863
1520-5126
DOI:10.1021/ja076210u