Rapid pulse length determination in high-resolution NMR

The 90°( 1H) pulse length can be determined in a single scan using a simple homo-gated decoupling/nutation experiment. We show that the method is fast, accurate and readily amenable to automation.

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Journal of magnetic resonance (1997) 2005-09, Vol.176 (1), p.115-119
Hauptverfasser: Wu, Peter S.C., Otting, Gottfried
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 119
container_issue 1
container_start_page 115
container_title Journal of magnetic resonance (1997)
container_volume 176
creator Wu, Peter S.C.
Otting, Gottfried
description The 90°( 1H) pulse length can be determined in a single scan using a simple homo-gated decoupling/nutation experiment. We show that the method is fast, accurate and readily amenable to automation.
doi_str_mv 10.1016/j.jmr.2005.05.018
format Article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_68485801</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S1090780705001837</els_id><sourcerecordid>68485801</sourcerecordid><originalsourceid>FETCH-LOGICAL-c351t-9c88ab13d22562ba1dbbbbf3cc8433aa971ef80391e593434a5017019b2820bd3</originalsourceid><addsrcrecordid>eNp9kFtLw0AQhRdRbK3-AF8kT76lzmS7yQafpHgDL1D0edlsJu2GXOpuIvjvTdqCbw4DMwznHJiPsUuEOQLGN-W8rN08AhDzsVEesSlCGocgRXy82yFMJCQTduZ9CYAoEjhlExRpEkUxn7Jkpbc2D7Z95SmoqFl3myCnjlxtG93ZtglsE2zsehM68m3V705vr6tzdlLowXNxmDP2-XD_sXwKX94fn5d3L6HhArswNVLqDHkeRSKOMo15NlTBjZELzrVOE6RCAk-RRMoXfKEFYAKYZpGMIMv5jF3vc7eu_erJd6q23lBV6Yba3qtYLqSQgIMQ90LjWu8dFWrrbK3dj0JQIy1VqoGWGmmpsVEOnqtDeJ_VlP85DngGwe1eQMOL35ac8sZSYyi3jkyn8tb-E_8LI4V5eg</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>68485801</pqid></control><display><type>article</type><title>Rapid pulse length determination in high-resolution NMR</title><source>MEDLINE</source><source>Elsevier ScienceDirect Journals</source><creator>Wu, Peter S.C. ; Otting, Gottfried</creator><creatorcontrib>Wu, Peter S.C. ; Otting, Gottfried</creatorcontrib><description>The 90°( 1H) pulse length can be determined in a single scan using a simple homo-gated decoupling/nutation experiment. We show that the method is fast, accurate and readily amenable to automation.</description><identifier>ISSN: 1090-7807</identifier><identifier>EISSN: 1096-0856</identifier><identifier>DOI: 10.1016/j.jmr.2005.05.018</identifier><identifier>PMID: 15972263</identifier><language>eng</language><publisher>United States: Elsevier Inc</publisher><subject>90° pulse ; Animals ; Automation ; Chickens ; Homo-gated decoupling ; Muramidase - chemistry ; Nuclear Magnetic Resonance, Biomolecular - methods ; Nutation spectroscopy</subject><ispartof>Journal of magnetic resonance (1997), 2005-09, Vol.176 (1), p.115-119</ispartof><rights>2005 Elsevier Inc.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c351t-9c88ab13d22562ba1dbbbbf3cc8433aa971ef80391e593434a5017019b2820bd3</citedby><cites>FETCH-LOGICAL-c351t-9c88ab13d22562ba1dbbbbf3cc8433aa971ef80391e593434a5017019b2820bd3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S1090780705001837$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/15972263$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Wu, Peter S.C.</creatorcontrib><creatorcontrib>Otting, Gottfried</creatorcontrib><title>Rapid pulse length determination in high-resolution NMR</title><title>Journal of magnetic resonance (1997)</title><addtitle>J Magn Reson</addtitle><description>The 90°( 1H) pulse length can be determined in a single scan using a simple homo-gated decoupling/nutation experiment. We show that the method is fast, accurate and readily amenable to automation.</description><subject>90° pulse</subject><subject>Animals</subject><subject>Automation</subject><subject>Chickens</subject><subject>Homo-gated decoupling</subject><subject>Muramidase - chemistry</subject><subject>Nuclear Magnetic Resonance, Biomolecular - methods</subject><subject>Nutation spectroscopy</subject><issn>1090-7807</issn><issn>1096-0856</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kFtLw0AQhRdRbK3-AF8kT76lzmS7yQafpHgDL1D0edlsJu2GXOpuIvjvTdqCbw4DMwznHJiPsUuEOQLGN-W8rN08AhDzsVEesSlCGocgRXy82yFMJCQTduZ9CYAoEjhlExRpEkUxn7Jkpbc2D7Z95SmoqFl3myCnjlxtG93ZtglsE2zsehM68m3V705vr6tzdlLowXNxmDP2-XD_sXwKX94fn5d3L6HhArswNVLqDHkeRSKOMo15NlTBjZELzrVOE6RCAk-RRMoXfKEFYAKYZpGMIMv5jF3vc7eu_erJd6q23lBV6Yba3qtYLqSQgIMQ90LjWu8dFWrrbK3dj0JQIy1VqoGWGmmpsVEOnqtDeJ_VlP85DngGwe1eQMOL35ac8sZSYyi3jkyn8tb-E_8LI4V5eg</recordid><startdate>20050901</startdate><enddate>20050901</enddate><creator>Wu, Peter S.C.</creator><creator>Otting, Gottfried</creator><general>Elsevier Inc</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20050901</creationdate><title>Rapid pulse length determination in high-resolution NMR</title><author>Wu, Peter S.C. ; Otting, Gottfried</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c351t-9c88ab13d22562ba1dbbbbf3cc8433aa971ef80391e593434a5017019b2820bd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>90° pulse</topic><topic>Animals</topic><topic>Automation</topic><topic>Chickens</topic><topic>Homo-gated decoupling</topic><topic>Muramidase - chemistry</topic><topic>Nuclear Magnetic Resonance, Biomolecular - methods</topic><topic>Nutation spectroscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wu, Peter S.C.</creatorcontrib><creatorcontrib>Otting, Gottfried</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of magnetic resonance (1997)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wu, Peter S.C.</au><au>Otting, Gottfried</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Rapid pulse length determination in high-resolution NMR</atitle><jtitle>Journal of magnetic resonance (1997)</jtitle><addtitle>J Magn Reson</addtitle><date>2005-09-01</date><risdate>2005</risdate><volume>176</volume><issue>1</issue><spage>115</spage><epage>119</epage><pages>115-119</pages><issn>1090-7807</issn><eissn>1096-0856</eissn><abstract>The 90°( 1H) pulse length can be determined in a single scan using a simple homo-gated decoupling/nutation experiment. We show that the method is fast, accurate and readily amenable to automation.</abstract><cop>United States</cop><pub>Elsevier Inc</pub><pmid>15972263</pmid><doi>10.1016/j.jmr.2005.05.018</doi><tpages>5</tpages></addata></record>
fulltext fulltext
identifier ISSN: 1090-7807
ispartof Journal of magnetic resonance (1997), 2005-09, Vol.176 (1), p.115-119
issn 1090-7807
1096-0856
language eng
recordid cdi_proquest_miscellaneous_68485801
source MEDLINE; Elsevier ScienceDirect Journals
subjects 90° pulse
Animals
Automation
Chickens
Homo-gated decoupling
Muramidase - chemistry
Nuclear Magnetic Resonance, Biomolecular - methods
Nutation spectroscopy
title Rapid pulse length determination in high-resolution NMR
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-28T22%3A52%3A43IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Rapid%20pulse%20length%20determination%20in%20high-resolution%20NMR&rft.jtitle=Journal%20of%20magnetic%20resonance%20(1997)&rft.au=Wu,%20Peter%20S.C.&rft.date=2005-09-01&rft.volume=176&rft.issue=1&rft.spage=115&rft.epage=119&rft.pages=115-119&rft.issn=1090-7807&rft.eissn=1096-0856&rft_id=info:doi/10.1016/j.jmr.2005.05.018&rft_dat=%3Cproquest_cross%3E68485801%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=68485801&rft_id=info:pmid/15972263&rft_els_id=S1090780705001837&rfr_iscdi=true