Rapid pulse length determination in high-resolution NMR

Rapid pulse length determination in high-resolution NMR

The 90°( 1H) pulse length can be determined in a single scan using a simple homo-gated decoupling/nutation experiment. We show that the method is fast, accurate and readily amenable to automation.

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Veröffentlicht in:Journal of magnetic resonance (1997) 2005-09, Vol.176 (1), p.115-119
Hauptverfasser: Wu, Peter S.C., Otting, Gottfried
Format: Artikel
Sprache:eng
Schlagworte:
90° pulse
Animals
Automation
Chickens
Homo-gated decoupling
Muramidase - chemistry
Nuclear Magnetic Resonance, Biomolecular - methods
Nutation spectroscopy
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Beschreibung
Zusammenfassung:The 90°( 1H) pulse length can be determined in a single scan using a simple homo-gated decoupling/nutation experiment. We show that the method is fast, accurate and readily amenable to automation.
ISSN:1090-7807
1096-0856
DOI:10.1016/j.jmr.2005.05.018