Analytical chemistry of synthetic routes to psychoactive tryptamines. Part I. Characterisation of the Speeter and Anthony synthetic route to 5-methoxy-N, N-diisopropyltryptamine using ESI-MS-MS and ESI-TOF-MS

5-Methoxy-N,N-diisopropyltryptamine (5-MeO-DIPT), a new psychoactive tryptamine derivative, has been synthesised by the Speeter and Anthony procedure. This synthetic route was characterised by ESI-MS-MS, ESI-TOF-MS and NMR. Side products have been identified as 3-(2-N,N-diisopropylamino-ethyl)-1H-in...

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Veröffentlicht in:	Analyst (London) 2004-01, Vol.129 (11), p.1047-1057
Hauptverfasser:	BRANDT, Simon D, FREEMAN, Sally, FLEET, Ian A, MCGAGH, Peter, ALDER, John F
Format:	Artikel
Sprache:	eng
Schlagworte:	5-Methoxytryptamine - analogs & derivatives 5-Methoxytryptamine - chemical synthesis 5-Methoxytryptamine - chemistry Analytical chemistry Chemistry Exact sciences and technology Magnetic Resonance Spectroscopy - methods Mass Spectrometry - methods Psychotropic Drugs - chemical synthesis Psychotropic Drugs - chemistry Spectrometric and optical methods Spectrometry, Mass, Electrospray Ionization - methods
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Beschreibung
Zusammenfassung:	5-Methoxy-N,N-diisopropyltryptamine (5-MeO-DIPT), a new psychoactive tryptamine derivative, has been synthesised by the Speeter and Anthony procedure. This synthetic route was characterised by ESI-MS-MS, ESI-TOF-MS and NMR. Side products have been identified as 3-(2-N,N-diisopropylamino-ethyl)-1H-indol-5-ol (5), 2-N,N-diisopropylamino-1-(5-methoxy-1H-indol-3-yl)-ethanol (6), 2-(5-methoxy-1H-indol-3-yl)-ethanol (7) and 2-N,N-diisopropylamino-1-(5-methoxy-1H-indol-3-yl)-ethanone (8).
ISSN:	0003-2654 1364-5528
DOI:	10.1039/b407239c