Influence of hot pressing on the microstructure and fracture toughness of two pressable dental glass-ceramics

Empress 1 and Empress 2 are well‐known pressable all‐ceramic dental materials that have generated substantial interest for many clinicians and patients. These two materials are reputed to benefit from heat pressing during the laboratory fabrication procedures, leading to better crystal distribution within a glass matrix, and hence an improved strength. The present study aimed to evaluate the effect of heat pressing on fracture toughness, microstructural features, and porosity. Results showed that Empress 1 had similar fracture toughness values before the pressing procedure, after it, and after the repressing procedure. The microstructural features were also similar among these specimens, but a more uniform distribution of leucite crystals was observed following the pressing and repressing procedures. Empress 2 demonstrated two different fracture toughness values. This was associated with the alignment of lithium disilicate crystals that occurred after the pressing and repressing procedures, which led to different indentation induced crack lengths, depending upon whether cracks propagated parallel to or perpendicular to the aligned crystals, the former having lower toughness than those that propagated in the perpendicular direction. Porosity, in terms of both the size and number of pores, was found to decrease after the pressing and repressing procedures for both materials. Repressing resulted in significant growth of the lithium disilicate crystals in Empress 2, but there was no change for the leucite crystals in Empress 1. The change in the lithium disilicate crystals' size did not have a noticeable effect on the fracture toughness of Empress 2. It was concluded that heat pressing did not significantly affect the fracture toughness of Empress 1, but resulted in two different values for Empress 2. It also decreased the size and number of pores for both materials, which could contribute to the strength improvement found after heat pressing, which has been reported in previous studies. © 2004 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater 71B: 99–107, 2004