Synthesis and study of sodium vanadomanganate
Sodium 13-vanadomanganate Na7[MnV13O38]DT5H2O (I) has been synthesized and studied by mass spectrometry, thermogravimetry, IR spectroscopy, and X-ray powder diffraction analysis. The crystals of compound I are monoclinic: a = 11.487 A, b = 7.613 A, c = 11.359 A, b = 114.15DG, V = 906.52 A, rcalcd =...
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Veröffentlicht in: | Russian journal of inorganic chemistry 2007-12, Vol.52 (12), p.1864-1867 |
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Hauptverfasser: | , , , , , |
Format: | Artikel |
Sprache: | eng |
Online-Zugang: | Volltext |
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Zusammenfassung: | Sodium 13-vanadomanganate Na7[MnV13O38]DT5H2O (I) has been synthesized and studied by mass spectrometry, thermogravimetry, IR spectroscopy, and X-ray powder diffraction analysis. The crystals of compound I are monoclinic: a = 11.487 A, b = 7.613 A, c = 11.359 A, b = 114.15DG, V = 906.52 A, rcalcd = 2.73 g/cm, Z = 1. |
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ISSN: | 0036-0236 1531-8613 |
DOI: | 10.1134/S0036023607120108 |