Preparation and characterization of magnetite/dextran nanocomposite used as a precursor of magnetic fluid

Magnetic nanoparticles were synthesized by the co-precipitation of Fe 2+ and Fe 3+ using ammonium hydroxide (NH 4OH). The obtained nanoparticles were characterized by X-ray powder diffraction, transmission electron microscopy, scanning electron microscopy, Fourier transform infrared (FT-IR) spectros...

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Veröffentlicht in:Chemical engineering journal (Lausanne, Switzerland : 1996) Switzerland : 1996), 2009-08, Vol.150 (2), p.572-580
Hauptverfasser: Hong, R.Y., Li, J.H., Qu, J.M., Chen, L.L., Li, H.Z.
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Sprache:eng
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Zusammenfassung:Magnetic nanoparticles were synthesized by the co-precipitation of Fe 2+ and Fe 3+ using ammonium hydroxide (NH 4OH). The obtained nanoparticles were characterized by X-ray powder diffraction, transmission electron microscopy, scanning electron microscopy, Fourier transform infrared (FT-IR) spectroscopy and vibrating sample magnetometer. In order to prepare a biocompatible water-based magnetic fluid, the nanoparticles were modified by dextran through a two-step method. The influences of dextran molecular weight on the size, morphology, coating efficiency and magnetic property of magnetite/dextran nanocomposite were investigated. The magnetite/dextran nanocomposite was dispersed in water to form a magnetic fluid by ball milling. The rheological property of magnetic fluids was investigated using a rotating rheometer.
ISSN:1385-8947
1873-3212
DOI:10.1016/j.cej.2009.03.034