Preparation and characterization of Ti-doped MgO nanopowders by a modified coprecipitation method

Ti-doped MgO nanopowders were prepared via a chemical coprecipitation method using acetic acid as a modifier in the presence of the surfactant polyethylene glycol (PEG 400). The as-obtained products were characterized by X-ray diffraction (XRD), X-ray fluorescence (XRF), differential thermal analysi...

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Veröffentlicht in:Journal of alloys and compounds 2008-08, Vol.461 (1), p.542-546
Hauptverfasser: Wang, Wei, Qiao, Xueliang, Chen, Jianguo, Tan, Fatang
Format: Artikel
Sprache:eng
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Zusammenfassung:Ti-doped MgO nanopowders were prepared via a chemical coprecipitation method using acetic acid as a modifier in the presence of the surfactant polyethylene glycol (PEG 400). The as-obtained products were characterized by X-ray diffraction (XRD), X-ray fluorescence (XRF), differential thermal analysis (DTA) and transmission electron microscopy (TEM). The results show that titanium atoms have been successfully incorporated into the crystal lattice of MgO with periclase structure. The modifier, acetic acid, can significantly reduce the particle size, and improve size distribution and dispersion of nanoparticles. In addition, the effect of doped titanium on the structure and morphology of magnesium oxide was also investigated.
ISSN:0925-8388
1873-4669
DOI:10.1016/j.jallcom.2007.07.046