Total Synthesis of Marine Oxylipins Solandelactones A-H

Total Synthesis of Marine Oxylipins Solandelactones A-H

The Solandelactones A–H have been synthesized via a short convergent approach utilizing common building blocks. Based on the diastereoselectivity of the crucial final addition step and on the comparison of prominent NMR data, a structural revision was necessary.

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Veröffentlicht in:Advanced synthesis & catalysis 2008-06, Vol.350 (9), p.1407-1412
Hauptverfasser: Pietruszka, Jörg, Rieche, Anja C. M.
Format: Artikel
Sprache:eng
Schlagworte:
asymmetric synthesis
cyclopropanes
natural products
structure elucidation
total synthesis
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Beschreibung
Zusammenfassung:The Solandelactones A–H have been synthesized via a short convergent approach utilizing common building blocks. Based on the diastereoselectivity of the crucial final addition step and on the comparison of prominent NMR data, a structural revision was necessary.
ISSN:1615-4150
1615-4169
DOI:10.1002/adsc.200800198