Synthesis of LSMO at low temperature by novel hydroxide precursor technique

A novel technique of mixing individual hydroxide is employed to prepare La0.65Sr0.35MnO3 (LSMO) at low temperature. Freshly prepared lanthanum and manganese hydroxides are mixed thoroughly with strontium hydroxide in stoichiometric ratio and heated at different temperatures ranging from 100 to 500 °...

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Veröffentlicht in:Materials letters 2008-02, Vol.62 (3), p.527-529
Hauptverfasser: Gupta, U.N., Muthurajan, H., Kumar, H.H., Koteswara Rao, N., Gokhale, S.P., Ravi, V.
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Sprache:eng
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Zusammenfassung:A novel technique of mixing individual hydroxide is employed to prepare La0.65Sr0.35MnO3 (LSMO) at low temperature. Freshly prepared lanthanum and manganese hydroxides are mixed thoroughly with strontium hydroxide in stoichiometric ratio and heated at different temperatures ranging from 100 to 500 °C for 6 h. At 500 °C, formation of La0.65Sr0.35MnO3 was confirmed by the X-ray diffraction studies (XRD). This is the lowest temperature so far reported in the literature. The particle size and morphology were investigated by scanning electron microscopy (SEM).
ISSN:0167-577X
1873-4979
DOI:10.1016/j.matlet.2007.05.077