Rapid analysis of pharmaceutical and personal care products by soft microwave-based plasma ionization—linear ion trap mass spectrometer (SMPI-LTQ) in natural water
In this study, a soft microwave plasma torch (SMPT) combined with a mass spectrometer (MS) was used for the first time as an analytical method to detect and analyze various pharmaceutical and personal care products (PPCPs) in aquatic environments without the need for sample pretreatment. For this pu...
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| Veröffentlicht in: | Environmental science and pollution research international 2023-10, Vol.30 (49), p.108263-108273 |
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| creator | Shuaibu, Nazifi Sani Zhao, Gaosheng Chu, Fengjian Wang, Xiaozhi |
| description | In this study, a soft microwave plasma torch (SMPT) combined with a mass spectrometer (MS) was used for the first time as an analytical method to detect and analyze various pharmaceutical and personal care products (PPCPs) in aquatic environments without the need for sample pretreatment. For this purpose, ambient SMPT was used to generate plasma for ionizing the analyte molecules. Accordingly, nine PPCPs were identified by the SMPT-MS, and their identification was verified by collision-induced dissociation (CID). The technique’s performance was verified with known PPCP samples, and the limits of detection (LOD) and quantification (LOQ) obtained over a linear range of 50–1 μg/L were 1.56 to 2.81 and 2.07 to 3.62 μg/L, respectively, with the standard addition recovery rate falling between 87.14 and 115.16%. These results show that the method has excellent sensitivity and selectivity, suggesting that SMPT can rapidly and directly detect PPCPs in environmental water, making it a promising method for rapid water quality inspection. |
| doi_str_mv | 10.1007/s11356-023-30018-5 |
| format | Article |
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For this purpose, ambient SMPT was used to generate plasma for ionizing the analyte molecules. Accordingly, nine PPCPs were identified by the SMPT-MS, and their identification was verified by collision-induced dissociation (CID). The technique’s performance was verified with known PPCP samples, and the limits of detection (LOD) and quantification (LOQ) obtained over a linear range of 50–1 μg/L were 1.56 to 2.81 and 2.07 to 3.62 μg/L, respectively, with the standard addition recovery rate falling between 87.14 and 115.16%. 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For this purpose, ambient SMPT was used to generate plasma for ionizing the analyte molecules. Accordingly, nine PPCPs were identified by the SMPT-MS, and their identification was verified by collision-induced dissociation (CID). The technique’s performance was verified with known PPCP samples, and the limits of detection (LOD) and quantification (LOQ) obtained over a linear range of 50–1 μg/L were 1.56 to 2.81 and 2.07 to 3.62 μg/L, respectively, with the standard addition recovery rate falling between 87.14 and 115.16%. 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Academic</collection><jtitle>Environmental science and pollution research international</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Shuaibu, Nazifi Sani</au><au>Zhao, Gaosheng</au><au>Chu, Fengjian</au><au>Wang, Xiaozhi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Rapid analysis of pharmaceutical and personal care products by soft microwave-based plasma ionization—linear ion trap mass spectrometer (SMPI-LTQ) in natural water</atitle><jtitle>Environmental science and pollution research international</jtitle><stitle>Environ Sci Pollut Res</stitle><date>2023-10-01</date><risdate>2023</risdate><volume>30</volume><issue>49</issue><spage>108263</spage><epage>108273</epage><pages>108263-108273</pages><issn>1614-7499</issn><issn>0944-1344</issn><eissn>1614-7499</eissn><abstract>In this study, a soft microwave plasma torch (SMPT) combined with a mass spectrometer (MS) was used for the first time as an analytical method to detect and analyze various pharmaceutical and personal care products (PPCPs) in aquatic environments without the need for sample pretreatment. For this purpose, ambient SMPT was used to generate plasma for ionizing the analyte molecules. Accordingly, nine PPCPs were identified by the SMPT-MS, and their identification was verified by collision-induced dissociation (CID). The technique’s performance was verified with known PPCP samples, and the limits of detection (LOD) and quantification (LOQ) obtained over a linear range of 50–1 μg/L were 1.56 to 2.81 and 2.07 to 3.62 μg/L, respectively, with the standard addition recovery rate falling between 87.14 and 115.16%. These results show that the method has excellent sensitivity and selectivity, suggesting that SMPT can rapidly and directly detect PPCPs in environmental water, making it a promising method for rapid water quality inspection.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s11356-023-30018-5</doi><tpages>11</tpages></addata></record> |
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| subjects | analytical methods Aquatic environment Aquatic Pollution Atmospheric Protection/Air Quality Control/Air Pollution Chemical wastewater Consumer products dissociation Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Ionization Mass spectrometers Microwave plasmas Personal grooming Pharmaceuticals rapid methods Research Article spectrometers Waste Water Technology Water Management Water Pollution Control Water quality |
| title | Rapid analysis of pharmaceutical and personal care products by soft microwave-based plasma ionization—linear ion trap mass spectrometer (SMPI-LTQ) in natural water |
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