Synthesis of Diaryl Ethers via Hypervalent Iodine-Mediated C–H Functionalization

A hypervalent iodine-reagent-based C–H functionalization strategy was utilized to synthesize diaryl ethers. This method directly transforms various arenes into their corresponding diaryliodonium salts, followed by a C–O coupling reaction to produce structurally diverse diaryl ethers. The efficacy of this approach in the late-stage structural modifications of complex molecules was demonstrated.