Growth and characterization of a novel nonlinear optical crystal zinc succinate, Zn(C 4H 4O 4)

The solubility–temperature curve of zinc (II) succinate in aqueous was measured, and the bulk single crystal of zinc (II) succinate in size 7×8×2 mm 3 has been successfully grown from aqueous solution by slow evaporation method. As-grown crystals were characterized by X-ray powder diffraction (XRPD)...

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Veröffentlicht in:	Journal of crystal growth 2007-10, Vol.308 (1), p.89-92
Hauptverfasser:	Pan, Jianguo, Zhang, Gongjun, Zheng, Yueqing, Lin, Jianli, Xu, Wei
Format:	Artikel
Sprache:	eng
Schlagworte:	A2. Growth from solutions A2. Single crystal growth B1. Zinc compounds B2. Nonlinear optic materials Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology Equations of state, phase equilibria, and phase transitions Exact sciences and technology Fundamental areas of phenomenology (including applications) Growth from solutions Materials science Methods of crystal growth physics of crystal growth Nonlinear optical crystals Optical materials Optics Physics Solubility, segregation, and mixing phase separation Theory and models of crystal growth physics of crystal growth, crystal morphology and orientation
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Zusammenfassung:	The solubility–temperature curve of zinc (II) succinate in aqueous was measured, and the bulk single crystal of zinc (II) succinate in size 7×8×2 mm 3 has been successfully grown from aqueous solution by slow evaporation method. As-grown crystals were characterized by X-ray powder diffraction (XRPD), Fourier transforms infrared spectroscopy (FTIR) and TG/DTA analyses. The second harmonic output intensity of Zn(C 4H 4O 4) was tested using the Kurtz and Perry method and was 6.5 times as large as KDP. UV–Vis–NIR spectrum shows excellent transmission through the visible region up to 1700 nm.
ISSN:	0022-0248 1873-5002
DOI:	10.1016/j.jcrysgro.2007.05.057