Fourier transform-based post-processing drift compensation and calibration method for scanning probe microscopy

Scanning probe microscopy (SPM) is ubiquitous in nanoscale science allowing the observation of features in real space down to the angstrom resolution. The scanning nature of SPM, wherein a sharp tip rasters the surface during which a physical setpoint is maintained via a control feedback loop, often...

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Veröffentlicht in:Ultramicroscopy 2024-09, Vol.263, p.113984, Article 113984
Hauptverfasser: Le Ster, M., Pawłowski, S., Lutsyk, I., Kowalczyk, P.J.
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Sprache:eng
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Zusammenfassung:Scanning probe microscopy (SPM) is ubiquitous in nanoscale science allowing the observation of features in real space down to the angstrom resolution. The scanning nature of SPM, wherein a sharp tip rasters the surface during which a physical setpoint is maintained via a control feedback loop, often implies that the image is subject to drift effects, leading to distortion of the resulting image. While there are in-operando methods to compensate for the drift, correcting the residual linear drift in obtained images is often neglected. In this paper, we present a reciprocal space-based technique to compensate the linear drift in atomically-resolved scanning probe microscopy images without distinction of the fast and slow scanning directions; furthermore this method does not require the set of SPM images obtained for the different scanning directions. Instead, the compensation is made possible by the a priori knowledge of the lattice parameters. The method can also be used to characterize and calibrate the SPM instrument. [Display omitted] •Scanning probe microscopy often suffers from distortion due to thermal drift.•Distortion is rationalized: bidirectional scaling, rotation and shear.•Present method compensates for drift for samples exhibiting periodic modulation.•Calibration of the instrument is also achieved with the present method.
ISSN:0304-3991
1879-2723
1879-2723
DOI:10.1016/j.ultramic.2024.113984