Ethyl acetate as an acetyl source and solvent for acetylation of alcohols by KOH

A KOH mediated mild, efficient, convenient and gram-scalable protocol for the acetylation of alcohols with EtOAc as acetyl source and solvent. Various types of alcohols were successfully transformed into according acetylated products. Good to excellent yields were offered by primary alcohols and low...

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Veröffentlicht in:RSC advances 2024-04, Vol.14 (18), p.12574-12579
Hauptverfasser: Wang, Xiaodan, Sun, Huilin, Cheng, Yao, Yang, Wenfei, Wang, Xinmei, Xiong, Liting, Li, Yiying, Wang, Jinhui, Gan, Chunli, Lin, Chunguang, Xu, Huanjun
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Sprache:eng
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Zusammenfassung:A KOH mediated mild, efficient, convenient and gram-scalable protocol for the acetylation of alcohols with EtOAc as acetyl source and solvent. Various types of alcohols were successfully transformed into according acetylated products. Good to excellent yields were offered by primary alcohols and low to moderate yields were offered by secondary alcohols. A mild, efficient and convenient procedure for the acetylation of alcohols with EtOAc as acetyl source and solvent mediated by KOH was reported.
ISSN:2046-2069
2046-2069
DOI:10.1039/d3ra08717d