Morphological evolution and characterization of hydrothermal synthesized Na2CuP2O7 crystals
Na2CuP2O7 crystals were synthesized by hydrothermal technique at moderate pressure-temperature conditions. The maximum degree of crystallinity is observed at critical concentration of initial components, beyond which the crystallinity collapses sharply to minimum. Solubility studies have revealed, p...
Gespeichert in:
| Veröffentlicht in: | Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2007-04, Vol.452-453, p.751-757 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 757 |
|---|---|
| container_issue | |
| container_start_page | 751 |
| container_title | Materials science & engineering. A, Structural materials : properties, microstructure and processing |
| container_volume | 452-453 |
| creator | MAHESH, M. J GOPALAKRISHNA, G. S ASHAMANJARI, K. G |
| description | Na2CuP2O7 crystals were synthesized by hydrothermal technique at moderate pressure-temperature conditions. The maximum degree of crystallinity is observed at critical concentration of initial components, beyond which the crystallinity collapses sharply to minimum. Solubility studies have revealed, positive thermal coefficient of solubility in a H3PO4 solvent with relatively high enthalpy. Thermal behaviour and structural coordination of the prepared materials were investigated, respectively, using DTA/TGA and FTIR measurements. Magnetic results have revealed; it is a frequency and temperature dependent prospective paramagnetic material. |
| doi_str_mv | 10.1016/j.msea.2006.10.135 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_29890621</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>29890621</sourcerecordid><originalsourceid>FETCH-LOGICAL-c308t-8eced3838aee109ea750868ea8937226c88f5257cc52702846765a76e2c1bb423</originalsourceid><addsrcrecordid>eNpFkDtPwzAcxC0EEqXwBZiywJbgR_waUcVLKpQBJobIdf4hqZK42AlS-ulJ2kpMdzrd3fBD6JrghGAi7jZJE8AkFGORTBnjJ2hGlGRxqpk4RTOsKYk51uwcXYSwwRiTFPMZ-np1flu62n1X1tQR_Lq67yrXRqbNI1sab2wHvtqZfeiKqBxy77oSfDPWw9CONlQ7yKM3Qxf9O13JyPohdKYOl-isGAWujjpHn48PH4vneLl6elncL2PLsOpiBRZyppgyAARrMJJjJRQYpZmkVFilCk65tJZTialKhRTcSAHUkvU6pWyObg-_W-9-eghd1lTBQl2bFlwfMqqVxoKSsUgPRetdCB6KbOurxvghIzibOGabbOKYTRz3GePj6Ob4bsKIqPCmtVX4XyquqZac_QE6IXVW</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>29890621</pqid></control><display><type>article</type><title>Morphological evolution and characterization of hydrothermal synthesized Na2CuP2O7 crystals</title><source>Elsevier ScienceDirect Journals</source><creator>MAHESH, M. J ; GOPALAKRISHNA, G. S ; ASHAMANJARI, K. G</creator><creatorcontrib>MAHESH, M. J ; GOPALAKRISHNA, G. S ; ASHAMANJARI, K. G</creatorcontrib><description>Na2CuP2O7 crystals were synthesized by hydrothermal technique at moderate pressure-temperature conditions. The maximum degree of crystallinity is observed at critical concentration of initial components, beyond which the crystallinity collapses sharply to minimum. Solubility studies have revealed, positive thermal coefficient of solubility in a H3PO4 solvent with relatively high enthalpy. Thermal behaviour and structural coordination of the prepared materials were investigated, respectively, using DTA/TGA and FTIR measurements. Magnetic results have revealed; it is a frequency and temperature dependent prospective paramagnetic material.</description><identifier>ISSN: 0921-5093</identifier><identifier>EISSN: 1873-4936</identifier><identifier>DOI: 10.1016/j.msea.2006.10.135</identifier><language>eng</language><publisher>Amsterdam: Elsevier</publisher><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties ; Cross-disciplinary physics: materials science; rheology ; Diamagnetism, paramagnetism and superparamagnetism ; Exact sciences and technology ; Growth from solutions ; Magnetic properties and materials ; Materials science ; Methods of crystal growth; physics of crystal growth ; Nonmetals ; Physics</subject><ispartof>Materials science & engineering. A, Structural materials : properties, microstructure and processing, 2007-04, Vol.452-453, p.751-757</ispartof><rights>2007 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c308t-8eced3838aee109ea750868ea8937226c88f5257cc52702846765a76e2c1bb423</citedby><cites>FETCH-LOGICAL-c308t-8eced3838aee109ea750868ea8937226c88f5257cc52702846765a76e2c1bb423</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=18592975$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>MAHESH, M. J</creatorcontrib><creatorcontrib>GOPALAKRISHNA, G. S</creatorcontrib><creatorcontrib>ASHAMANJARI, K. G</creatorcontrib><title>Morphological evolution and characterization of hydrothermal synthesized Na2CuP2O7 crystals</title><title>Materials science & engineering. A, Structural materials : properties, microstructure and processing</title><description>Na2CuP2O7 crystals were synthesized by hydrothermal technique at moderate pressure-temperature conditions. The maximum degree of crystallinity is observed at critical concentration of initial components, beyond which the crystallinity collapses sharply to minimum. Solubility studies have revealed, positive thermal coefficient of solubility in a H3PO4 solvent with relatively high enthalpy. Thermal behaviour and structural coordination of the prepared materials were investigated, respectively, using DTA/TGA and FTIR measurements. Magnetic results have revealed; it is a frequency and temperature dependent prospective paramagnetic material.</description><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Diamagnetism, paramagnetism and superparamagnetism</subject><subject>Exact sciences and technology</subject><subject>Growth from solutions</subject><subject>Magnetic properties and materials</subject><subject>Materials science</subject><subject>Methods of crystal growth; physics of crystal growth</subject><subject>Nonmetals</subject><subject>Physics</subject><issn>0921-5093</issn><issn>1873-4936</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNpFkDtPwzAcxC0EEqXwBZiywJbgR_waUcVLKpQBJobIdf4hqZK42AlS-ulJ2kpMdzrd3fBD6JrghGAi7jZJE8AkFGORTBnjJ2hGlGRxqpk4RTOsKYk51uwcXYSwwRiTFPMZ-np1flu62n1X1tQR_Lq67yrXRqbNI1sab2wHvtqZfeiKqBxy77oSfDPWw9CONlQ7yKM3Qxf9O13JyPohdKYOl-isGAWujjpHn48PH4vneLl6elncL2PLsOpiBRZyppgyAARrMJJjJRQYpZmkVFilCk65tJZTialKhRTcSAHUkvU6pWyObg-_W-9-eghd1lTBQl2bFlwfMqqVxoKSsUgPRetdCB6KbOurxvghIzibOGabbOKYTRz3GePj6Ob4bsKIqPCmtVX4XyquqZac_QE6IXVW</recordid><startdate>20070415</startdate><enddate>20070415</enddate><creator>MAHESH, M. J</creator><creator>GOPALAKRISHNA, G. S</creator><creator>ASHAMANJARI, K. G</creator><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20070415</creationdate><title>Morphological evolution and characterization of hydrothermal synthesized Na2CuP2O7 crystals</title><author>MAHESH, M. J ; GOPALAKRISHNA, G. S ; ASHAMANJARI, K. G</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c308t-8eced3838aee109ea750868ea8937226c88f5257cc52702846765a76e2c1bb423</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Condensed matter: electronic structure, electrical, magnetic, and optical properties</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Diamagnetism, paramagnetism and superparamagnetism</topic><topic>Exact sciences and technology</topic><topic>Growth from solutions</topic><topic>Magnetic properties and materials</topic><topic>Materials science</topic><topic>Methods of crystal growth; physics of crystal growth</topic><topic>Nonmetals</topic><topic>Physics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>MAHESH, M. J</creatorcontrib><creatorcontrib>GOPALAKRISHNA, G. S</creatorcontrib><creatorcontrib>ASHAMANJARI, K. G</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>MAHESH, M. J</au><au>GOPALAKRISHNA, G. S</au><au>ASHAMANJARI, K. G</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Morphological evolution and characterization of hydrothermal synthesized Na2CuP2O7 crystals</atitle><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle><date>2007-04-15</date><risdate>2007</risdate><volume>452-453</volume><spage>751</spage><epage>757</epage><pages>751-757</pages><issn>0921-5093</issn><eissn>1873-4936</eissn><abstract>Na2CuP2O7 crystals were synthesized by hydrothermal technique at moderate pressure-temperature conditions. The maximum degree of crystallinity is observed at critical concentration of initial components, beyond which the crystallinity collapses sharply to minimum. Solubility studies have revealed, positive thermal coefficient of solubility in a H3PO4 solvent with relatively high enthalpy. Thermal behaviour and structural coordination of the prepared materials were investigated, respectively, using DTA/TGA and FTIR measurements. Magnetic results have revealed; it is a frequency and temperature dependent prospective paramagnetic material.</abstract><cop>Amsterdam</cop><pub>Elsevier</pub><doi>10.1016/j.msea.2006.10.135</doi><tpages>7</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0921-5093 |
| ispartof | Materials science & engineering. A, Structural materials : properties, microstructure and processing, 2007-04, Vol.452-453, p.751-757 |
| issn | 0921-5093 1873-4936 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_29890621 |
| source | Elsevier ScienceDirect Journals |
| subjects | Condensed matter: electronic structure, electrical, magnetic, and optical properties Cross-disciplinary physics: materials science rheology Diamagnetism, paramagnetism and superparamagnetism Exact sciences and technology Growth from solutions Magnetic properties and materials Materials science Methods of crystal growth physics of crystal growth Nonmetals Physics |
| title | Morphological evolution and characterization of hydrothermal synthesized Na2CuP2O7 crystals |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-10T00%3A28%3A46IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Morphological%20evolution%20and%20characterization%20of%20hydrothermal%20synthesized%20Na2CuP2O7%20crystals&rft.jtitle=Materials%20science%20&%20engineering.%20A,%20Structural%20materials%20:%20properties,%20microstructure%20and%20processing&rft.au=MAHESH,%20M.%20J&rft.date=2007-04-15&rft.volume=452-453&rft.spage=751&rft.epage=757&rft.pages=751-757&rft.issn=0921-5093&rft.eissn=1873-4936&rft_id=info:doi/10.1016/j.msea.2006.10.135&rft_dat=%3Cproquest_cross%3E29890621%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=29890621&rft_id=info:pmid/&rfr_iscdi=true |