Preparation and characterisation of carbon-coated ceramic foams for organic vapour adsorption
Ceramic foam substrates of various porosities were coated with novolak resin, which was then subsequently carbonised and activated to develop a pore structure. The carbon forming the layer was characterised by thermal analysis, TPD and N 2, CO 2 and hexane vapour adsorption. It was found to be micro...
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Veröffentlicht in: | Carbon (New York) 2006-06, Vol.44 (7), p.1189-1197 |
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Hauptverfasser: | , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Ceramic foam substrates of various porosities were coated with novolak resin, which was then subsequently carbonised and activated to develop a pore structure. The carbon forming the layer was characterised by thermal analysis, TPD and N
2, CO
2 and hexane vapour adsorption. It was found to be microporous with a high surface area (up to 1400
m
2
g
−1), which made it a good adsorbent for hexane vapour at ambient temperature. The carbon–ceramic interface was examined using SEM. The coated foams displayed a reduced pressure drop compared to carbon granules and had good dynamic hexane vapour adsorption characteristics. Depending on the foam architecture, hexane breakthrough was delayed for up to 78
min. |
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ISSN: | 0008-6223 1873-3891 |
DOI: | 10.1016/j.carbon.2005.10.053 |