Dissipation kinetics, decontamination, consumer risk assessment and monitoring of flonicamid and imidacloprid residues in capsicum under open field and polyhouse condition

Liquid chromatography mass spectrometry (LC-MS)-based detection of flonicamid, imidacloprid and 6-chloronicotinic acid residues was validated and analysed in capsicum fruit, processed products and soil. The standard concentrations (0.0025 to 0.25 μg mL −1 ) of insecticides had a good linear curve (...

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Veröffentlicht in:Environmental science and pollution research international 2023-11, Vol.30 (54), p.116039-116051
Hauptverfasser: Subasekaran, Raghul, Kaithamalai, Bhuvaneswari, Angappan, Suganthi, Thiruvenkatasamy, Saraswathi, Narayanan, Maragatham
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Sprache:eng
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Zusammenfassung:Liquid chromatography mass spectrometry (LC-MS)-based detection of flonicamid, imidacloprid and 6-chloronicotinic acid residues was validated and analysed in capsicum fruit, processed products and soil. The standard concentrations (0.0025 to 0.25 μg mL −1 ) of insecticides had a good linear curve ( r 2 >0.99). Limit of detection and limit of quantification values were 0.0025 and 0.01 mg kg −1 , respectively. The accuracy (80.53 to 100.33 %) of capsicum matrices and soil (89.41 to 100.52 %) and precision (RSD
ISSN:1614-7499
0944-1344
1614-7499
DOI:10.1007/s11356-023-30522-8