Dissipation kinetics, decontamination, consumer risk assessment and monitoring of flonicamid and imidacloprid residues in capsicum under open field and polyhouse condition
Liquid chromatography mass spectrometry (LC-MS)-based detection of flonicamid, imidacloprid and 6-chloronicotinic acid residues was validated and analysed in capsicum fruit, processed products and soil. The standard concentrations (0.0025 to 0.25 μg mL −1 ) of insecticides had a good linear curve (...
Gespeichert in:
Veröffentlicht in: | Environmental science and pollution research international 2023-11, Vol.30 (54), p.116039-116051 |
---|---|
Hauptverfasser: | , , , , |
Format: | Artikel |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | Liquid chromatography mass spectrometry (LC-MS)-based detection of flonicamid, imidacloprid and 6-chloronicotinic acid residues was validated and analysed in capsicum fruit, processed products and soil. The standard concentrations (0.0025 to 0.25 μg mL
−1
) of insecticides had a good linear curve (
r
2
>0.99). Limit of detection and limit of quantification values were 0.0025 and 0.01 mg kg
−1
, respectively. The accuracy (80.53 to 100.33 %) of capsicum matrices and soil (89.41 to 100.52 %) and precision (RSD |
---|---|
ISSN: | 1614-7499 0944-1344 1614-7499 |
DOI: | 10.1007/s11356-023-30522-8 |