Low temperature synthesis of boron phosphide nanocrystals

Nanocrystalline boron phosphide (BP) was successfully synthesized at low temperature (400 °C) by a simple reaction between PCl 3 and NaBF 4 using Na as reductant. X-ray powder diffraction patterns indicated that the resultant was cubic BP with a lattice constant a=4.533 Å. Transmission electron micr...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Materials letters 2005-04, Vol.59 (8), p.865-867
Hauptverfasser: Feng, Xin, Shi, Li-Yi, Hang, Jian-Zhong, Zhang, Jian-Ping, Fang, Jian-Hui, Zhong, Qing-Dong
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 867
container_issue 8
container_start_page 865
container_title Materials letters
container_volume 59
creator Feng, Xin
Shi, Li-Yi
Hang, Jian-Zhong
Zhang, Jian-Ping
Fang, Jian-Hui
Zhong, Qing-Dong
description Nanocrystalline boron phosphide (BP) was successfully synthesized at low temperature (400 °C) by a simple reaction between PCl 3 and NaBF 4 using Na as reductant. X-ray powder diffraction patterns indicated that the resultant was cubic BP with a lattice constant a=4.533 Å. Transmission electron microscopy revealed that the crystals were composed of spherical particles with the diameter of 80 nm or so and lots of worm-like rods. The possible formation mechanism was also investigated.
doi_str_mv 10.1016/j.matlet.2004.10.067
format Article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_28549174</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S0167577X0400895X</els_id><sourcerecordid>28549174</sourcerecordid><originalsourceid>FETCH-LOGICAL-c403t-36176c170d938513a18148364a58e6418a888d8d79086f2093c0c7916f76be533</originalsourceid><addsrcrecordid>eNp9kE1LxDAURYMoOI7-AxdduWtNJmk-NoIMOgoFNwruQiZ9ZTK0TU0yyvx7M9S1qweXcy-8g9AtwRXBhN_vq8GkHlK1wpjlqMJcnKEFkYKWTAl1jhYZE2UtxOcluopxjzOoMFsg1fifIsEwQTDpEKCIxzHtILpY-K7Y-uDHYtr5OO1cC8VoRm_DMSbTx2t00eUDN393iT6en97XL2XztnldPzalZZimknIiuCUCt4rKmlBDJGGScmZqCZwRaaSUrWyFwpJ3K6yoxVYowjvBt1BTukR38-4U_NcBYtKDixb63ozgD1GvZM0UESyDbAZt8DEG6PQU3GDCUROsT570Xs-e9MnTKc2ecu1hrkF-4ttB0NE6GC20LoBNuvXu_4FfZIdyKw</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>28549174</pqid></control><display><type>article</type><title>Low temperature synthesis of boron phosphide nanocrystals</title><source>Elsevier ScienceDirect Journals Complete</source><creator>Feng, Xin ; Shi, Li-Yi ; Hang, Jian-Zhong ; Zhang, Jian-Ping ; Fang, Jian-Hui ; Zhong, Qing-Dong</creator><creatorcontrib>Feng, Xin ; Shi, Li-Yi ; Hang, Jian-Zhong ; Zhang, Jian-Ping ; Fang, Jian-Hui ; Zhong, Qing-Dong</creatorcontrib><description>Nanocrystalline boron phosphide (BP) was successfully synthesized at low temperature (400 °C) by a simple reaction between PCl 3 and NaBF 4 using Na as reductant. X-ray powder diffraction patterns indicated that the resultant was cubic BP with a lattice constant a=4.533 Å. Transmission electron microscopy revealed that the crystals were composed of spherical particles with the diameter of 80 nm or so and lots of worm-like rods. The possible formation mechanism was also investigated.</description><identifier>ISSN: 0167-577X</identifier><identifier>EISSN: 1873-4979</identifier><identifier>DOI: 10.1016/j.matlet.2004.10.067</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Boron phosphide ; Nanomaterials ; Semiconductors ; Transmission electron microscopy ; X-ray techniques</subject><ispartof>Materials letters, 2005-04, Vol.59 (8), p.865-867</ispartof><rights>2004 Elsevier B.V.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c403t-36176c170d938513a18148364a58e6418a888d8d79086f2093c0c7916f76be533</citedby><cites>FETCH-LOGICAL-c403t-36176c170d938513a18148364a58e6418a888d8d79086f2093c0c7916f76be533</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.matlet.2004.10.067$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,777,781,3537,27905,27906,45976</link.rule.ids></links><search><creatorcontrib>Feng, Xin</creatorcontrib><creatorcontrib>Shi, Li-Yi</creatorcontrib><creatorcontrib>Hang, Jian-Zhong</creatorcontrib><creatorcontrib>Zhang, Jian-Ping</creatorcontrib><creatorcontrib>Fang, Jian-Hui</creatorcontrib><creatorcontrib>Zhong, Qing-Dong</creatorcontrib><title>Low temperature synthesis of boron phosphide nanocrystals</title><title>Materials letters</title><description>Nanocrystalline boron phosphide (BP) was successfully synthesized at low temperature (400 °C) by a simple reaction between PCl 3 and NaBF 4 using Na as reductant. X-ray powder diffraction patterns indicated that the resultant was cubic BP with a lattice constant a=4.533 Å. Transmission electron microscopy revealed that the crystals were composed of spherical particles with the diameter of 80 nm or so and lots of worm-like rods. The possible formation mechanism was also investigated.</description><subject>Boron phosphide</subject><subject>Nanomaterials</subject><subject>Semiconductors</subject><subject>Transmission electron microscopy</subject><subject>X-ray techniques</subject><issn>0167-577X</issn><issn>1873-4979</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><recordid>eNp9kE1LxDAURYMoOI7-AxdduWtNJmk-NoIMOgoFNwruQiZ9ZTK0TU0yyvx7M9S1qweXcy-8g9AtwRXBhN_vq8GkHlK1wpjlqMJcnKEFkYKWTAl1jhYZE2UtxOcluopxjzOoMFsg1fifIsEwQTDpEKCIxzHtILpY-K7Y-uDHYtr5OO1cC8VoRm_DMSbTx2t00eUDN393iT6en97XL2XztnldPzalZZimknIiuCUCt4rKmlBDJGGScmZqCZwRaaSUrWyFwpJ3K6yoxVYowjvBt1BTukR38-4U_NcBYtKDixb63ozgD1GvZM0UESyDbAZt8DEG6PQU3GDCUROsT570Xs-e9MnTKc2ecu1hrkF-4ttB0NE6GC20LoBNuvXu_4FfZIdyKw</recordid><startdate>20050401</startdate><enddate>20050401</enddate><creator>Feng, Xin</creator><creator>Shi, Li-Yi</creator><creator>Hang, Jian-Zhong</creator><creator>Zhang, Jian-Ping</creator><creator>Fang, Jian-Hui</creator><creator>Zhong, Qing-Dong</creator><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20050401</creationdate><title>Low temperature synthesis of boron phosphide nanocrystals</title><author>Feng, Xin ; Shi, Li-Yi ; Hang, Jian-Zhong ; Zhang, Jian-Ping ; Fang, Jian-Hui ; Zhong, Qing-Dong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c403t-36176c170d938513a18148364a58e6418a888d8d79086f2093c0c7916f76be533</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>Boron phosphide</topic><topic>Nanomaterials</topic><topic>Semiconductors</topic><topic>Transmission electron microscopy</topic><topic>X-ray techniques</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Feng, Xin</creatorcontrib><creatorcontrib>Shi, Li-Yi</creatorcontrib><creatorcontrib>Hang, Jian-Zhong</creatorcontrib><creatorcontrib>Zhang, Jian-Ping</creatorcontrib><creatorcontrib>Fang, Jian-Hui</creatorcontrib><creatorcontrib>Zhong, Qing-Dong</creatorcontrib><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Materials letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Feng, Xin</au><au>Shi, Li-Yi</au><au>Hang, Jian-Zhong</au><au>Zhang, Jian-Ping</au><au>Fang, Jian-Hui</au><au>Zhong, Qing-Dong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Low temperature synthesis of boron phosphide nanocrystals</atitle><jtitle>Materials letters</jtitle><date>2005-04-01</date><risdate>2005</risdate><volume>59</volume><issue>8</issue><spage>865</spage><epage>867</epage><pages>865-867</pages><issn>0167-577X</issn><eissn>1873-4979</eissn><abstract>Nanocrystalline boron phosphide (BP) was successfully synthesized at low temperature (400 °C) by a simple reaction between PCl 3 and NaBF 4 using Na as reductant. X-ray powder diffraction patterns indicated that the resultant was cubic BP with a lattice constant a=4.533 Å. Transmission electron microscopy revealed that the crystals were composed of spherical particles with the diameter of 80 nm or so and lots of worm-like rods. The possible formation mechanism was also investigated.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.matlet.2004.10.067</doi><tpages>3</tpages></addata></record>
fulltext fulltext
identifier ISSN: 0167-577X
ispartof Materials letters, 2005-04, Vol.59 (8), p.865-867
issn 0167-577X
1873-4979
language eng
recordid cdi_proquest_miscellaneous_28549174
source Elsevier ScienceDirect Journals Complete
subjects Boron phosphide
Nanomaterials
Semiconductors
Transmission electron microscopy
X-ray techniques
title Low temperature synthesis of boron phosphide nanocrystals
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-17T15%3A02%3A14IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Low%20temperature%20synthesis%20of%20boron%20phosphide%20nanocrystals&rft.jtitle=Materials%20letters&rft.au=Feng,%20Xin&rft.date=2005-04-01&rft.volume=59&rft.issue=8&rft.spage=865&rft.epage=867&rft.pages=865-867&rft.issn=0167-577X&rft.eissn=1873-4979&rft_id=info:doi/10.1016/j.matlet.2004.10.067&rft_dat=%3Cproquest_cross%3E28549174%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=28549174&rft_id=info:pmid/&rft_els_id=S0167577X0400895X&rfr_iscdi=true