Change of Young's modulus of cold-deformed pure iron in a tensile test

Changes in Young's modulus E (determined according to ASTM E-111) of polycrystalline pure iron deformed by a tensile test at room temperature are determined. From its original mean value, 210 GPa. E decreased with deformation to a mean value of 196 GPa at ε = 0.060. Thereafter, slight recovery occurred and E stabilized to 198 GPa until the appearance of neck (ε = 0.100). With the aim to examine the causes of this behavior, residual stresses and textures were measured and the dislocation structure was observed by transmission electron microscopy (TEM). Longitudinal residual stresses increased from the first step of deformation (ε = 0.015) and remained constant until the samples fractured. There was no significant difference in texture throughout the deformation process, during which the increment of α fiber was smooth. Thus, the decrease of E cannot be attributed to residual stresses or textures. A relationship between dislocation arrangement and decrease off is proposed. Following the model established by Mott, dislocations can bow out in their glide planes, giving extra elastic strain and thus a decrease of E. The increase of the dislocation density during the first steps of deformation lowers the E values, since the extra elastic strain increases. At higher strains, when the cellular dislocation structure has formed (between ε = 0.060 and 0.080). the dislocations in cell interiors are capable of giving an extra elasticstrain, whereas the dislocations trapped in the cell walls are not. However, the dislocation density in cell interiors is lower than the dislocation density in the early stages of deformation in which the cell structure has not been developed. This produces the slight recovery of E measured at these strains. From ε = 0.080, the values of E stabilized since no changes in dislocation density in cell interiors are observed. [PUBLICATION ABSTRACT]