The synthesis of CU3BiS3 nanorods via a simple ethanol-thermal route

Cu3BiS3 nanorods with different aspect ratios were obtained via simple ethanol-thermal reactions between CuCl2-2H2O, BiCl3 and thiourea at relatively low temperature (160DGC, 10h). The as-prepared samples were characterized by means of X-ray powder diffraction, transmission electron microscopy, and...

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Veröffentlicht in:Journal of crystal growth 2003-06, Vol.253 (1-4), p.512-516
Hauptverfasser: Chen, Di, Shen, Guozhen, Tang, Kaibin, Liu, Xianming, Qian, Yitai, Zhou, Guien
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Sprache:eng
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Zusammenfassung:Cu3BiS3 nanorods with different aspect ratios were obtained via simple ethanol-thermal reactions between CuCl2-2H2O, BiCl3 and thiourea at relatively low temperature (160DGC, 10h). The as-prepared samples were characterized by means of X-ray powder diffraction, transmission electron microscopy, and X-ray photoelectron spectra. Studies found that the solvent has great influence on the aspect ratio of as-prepared Cu3BiS3 nanorods.
ISSN:0022-0248
1873-5002
DOI:10.1016/s0022-0248(03)01108-4