Rapid synthesis of nanocrystalline SnO2 powders by microwave heating method

Rapid synthesis of nanocrystalline SnO2 powders by microwave heating method

Nanocrystalline SnO2 powders of about 3 nm in size were prepared by a microwave irradiation heating technique from an aqueous solution in the presence of SnCl4 and urea. The particles were characterised by TEM, XRD, DSC, TG and reflectance spectra. A band gap is estimated to be 4.5 eV from the optic...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Materials letters 2002-03, Vol.53 (1-2), p.12-19
Hauptverfasser: ZHU, Jun-Jie, ZHU, Jian-Min, LIAO, Xue-Hong, FANG, Jiang-Lin, ZHOU, Miao-Gao, CHEN, Hong-Yuan
Format: Artikel
Sprache:eng
Schlagworte:
Cross-disciplinary physics: materials science
rheology
Exact sciences and technology
Materials science
Nanoscale materials and structures: fabrication and characterization
Physics
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:Nanocrystalline SnO2 powders of about 3 nm in size were prepared by a microwave irradiation heating technique from an aqueous solution in the presence of SnCl4 and urea. The particles were characterised by TEM, XRD, DSC, TG and reflectance spectra. A band gap is estimated to be 4.5 eV from the optical measurement of the nanoparticles. 47 refs.
ISSN:0167-577X
1873-4979
DOI:10.1016/s0167-577x(01)00445-1