Dilatometry study of the sintering behavior of boron-alloyed Fe-1.5 Pct Mo powder
The effect of different boron concentrations on the sintering behavior of an Fe-1.5 pct Mo (wt pct) prealloyed powder was investigated. Sintering was carried out in a dilatometer so that all dimensional changes involved with the densification process could be followed. Several transformations were f...
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Veröffentlicht in: | Metallurgical and materials transactions. A, Physical metallurgy and materials science Physical metallurgy and materials science, 2000-06, Vol.31 (6), p.1497-1506 |
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Sprache: | eng |
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Zusammenfassung: | The effect of different boron concentrations on the sintering behavior of an Fe-1.5 pct Mo (wt pct) prealloyed powder was investigated. Sintering was carried out in a dilatometer so that all dimensional changes involved with the densification process could be followed. Several transformations were found to occur by heating powder compacts to 1200 C and then cooling them to room temperature. At high temperatures, boron promoted the formation of liquid phases that, through a more-efficient sintering kinetics, promoted a satisfactory densification. Faster heating rates also had beneficial effects on the density of the final products. From a microstructural point of view, boron tended to destabilize the ferritic phase and to form iron and molybdenum borides. These borides can be found both in the intergranular regions, with a typical eutectic morphology, and dispersed in the ferritic matrix, in the form of nanometer-sized precipitates. This feature, having a significant effect on the hardness of the bulk material, has been ascribed to a bainite-like precipitation of borides from an undercooled austenitic phase. (Author) |
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ISSN: | 1073-5623 1543-1940 |
DOI: | 10.1007/s11661-000-0160-9 |