Comprehensive analysis of polyphenols from hybrid Mandarin peels by SPE and HPLC-UV

Polyphenol compounds are the most important bioactive components in citrus peels. An efficient clean-up method based on solid-phase extraction with C₁₈ cartridges (SPE-C₁₈) and high-performance liquid chromatography, coupled with ultraviolet detector (HPLC-UV) determination, was set up for the analy...

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Veröffentlicht in:Food science & technology 2022-08, Vol.165, p.113770, Article 113770
Hauptverfasser: Anticona, Mayra, Lopez-Malo, Daniel, Frigola, Ana, Esteve, Maria Jose, Blesa, Jesus
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Sprache:eng
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Zusammenfassung:Polyphenol compounds are the most important bioactive components in citrus peels. An efficient clean-up method based on solid-phase extraction with C₁₈ cartridges (SPE-C₁₈) and high-performance liquid chromatography, coupled with ultraviolet detector (HPLC-UV) determination, was set up for the analysis of phenolic composition in ultrasound assisted extraction from hybrid mandarin (Citrus reticulata) peels (Clemenvilla, Nadorcott, Ortanique). The SPE-C₁₈/HPLC-UV method was validated according to linearity (R² ≥ 0.998), good precision (intra-day and inter-day), relative standard deviations (
ISSN:0023-6438
DOI:10.1016/j.lwt.2022.113770