Dendritic morphologies of directionally solidified single crystals along different crystallographic orientations

Pb-2.2 wt% Sb alloy was directionally solidified along [1 0 0], [1 1 0] and [1 1 1] crystallographic orientations using pure lead single crystal seeds, with a positive thermal gradient of 140 K cm −1 and growth rate of 10 μm s −1, and then quenched. Longitudinal (parallel to the growth direction) an...

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Veröffentlicht in:Journal of crystal growth 2002-03, Vol.236 (1), p.420-428
Hauptverfasser: Ding, G.L, Tewari, S.N
Format: Artikel
Sprache:eng
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Zusammenfassung:Pb-2.2 wt% Sb alloy was directionally solidified along [1 0 0], [1 1 0] and [1 1 1] crystallographic orientations using pure lead single crystal seeds, with a positive thermal gradient of 140 K cm −1 and growth rate of 10 μm s −1, and then quenched. Longitudinal (parallel to the growth direction) and transverse microstructures in the mushy region and in the quenched portion ahead of the solidification front were examined to investigate the morphology of primary dendrites solidified along different crystallographic orientations. Transverse microstructures showed that for growth along [1 0 0] the primary dendrites had the usual four-fold symmetry due to side-branching; for [1 1 0] orientation, they appeared plate like; while for [1 1 1] orientation, a uniform distribution of nodes was observed. These observations confirm that side-branches in FCC metal alloys grow along 〈1 0 0〉 crystallographic directions irrespective of heat-extraction direction.
ISSN:0022-0248
1873-5002
DOI:10.1016/S0022-0248(01)01787-0