Real surface determination of Co sub(3)O sub(4) by Zn super(2+) adsorption. A comparison between x-ray diffraction, cyclic voltammetry and adsorption methods
The real surface areas of Co sub(3)O sub(4) films have been measured by Zn super(2+) adsorption. Co sub(3)O sub(4) films have been prepared by spray pyrolysis. The results are compared with crystallite sizes obtained by X-ray diffraction measurements and roughness factors calculated from cyclic volt...
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Veröffentlicht in: | Electrochimica acta 1998-01, Vol.43 (8), p.893-898 |
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Hauptverfasser: | , , , , , |
Format: | Artikel |
Sprache: | eng |
Online-Zugang: | Volltext |
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Zusammenfassung: | The real surface areas of Co sub(3)O sub(4) films have been measured by Zn super(2+) adsorption. Co sub(3)O sub(4) films have been prepared by spray pyrolysis. The results are compared with crystallite sizes obtained by X-ray diffraction measurements and roughness factors calculated from cyclic voltammograms. Discrepancies between the three methods are discussed and examined. |
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ISSN: | 0013-4686 |