Characterization of polyamide 6 made by reactive extrusion. II. Analysis of microstructure

Characterization of polyamide 6 made by reactive extrusion. II. Analysis of microstructure

Consideration is given to the characterization of microstructure in polyamide 6 prepared by polymerization of ϵ‐caprolactam in a corotating twin‐screw extruder. Results obtained by FTIR, WAXD, DSC, and DMTA are discussed in terms of the molecular mass of the polymer, the thermal history of the mater...

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Veröffentlicht in:Journal of applied polymer science 1994-11, Vol.54 (7), p.899-907
Hauptverfasser: Hornsby, P. R., Tung, J. F.
Format: Artikel
Sprache:eng
Schlagworte:
Applied sciences
Exact sciences and technology
Organic polymers
Physicochemistry of polymers
Properties and characterization
Structure, morphology and analysis
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Zusammenfassung:Consideration is given to the characterization of microstructure in polyamide 6 prepared by polymerization of ϵ‐caprolactam in a corotating twin‐screw extruder. Results obtained by FTIR, WAXD, DSC, and DMTA are discussed in terms of the molecular mass of the polymer, the thermal history of the material, and the influence of residual monomer. © 1994 John Wiley & Sons, Inc.
ISSN:0021-8995
1097-4628
DOI:10.1002/app.1994.070540709