Ultrafine Spinel Powders by Flame Spray Pyrolysis of a Magnesium Aluminum Double Alkoxide

Ultrafine crystalline spinel powder has been prepared using flame spray pyrolysis of alcoholic solutions of a novel double alkoxide precursor. The particles produced are spherical, dense, single crystals with diameters of 10–100 nm and specific surface areas ranging from 40 to 60 m2/g. Powder produc...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Journal of the American Ceramic Society 1996-05, Vol.79 (5), p.1419-1423
Hauptverfasser: Bickmore, Clint R., Waldner, Kurt F., Treadwell, David R., Laine, Richard M.
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:Ultrafine crystalline spinel powder has been prepared using flame spray pyrolysis of alcoholic solutions of a novel double alkoxide precursor. The particles produced are spherical, dense, single crystals with diameters of 10–100 nm and specific surface areas ranging from 40 to 60 m2/g. Powder production rates of 50–100 g/h are achieved using a bench‐top apparatus. Particle formation appears to occur by rapid oxidation of the organic ligands followed by nucleation and growth from oxide species.
ISSN:0002-7820
1551-2916
DOI:10.1111/j.1151-2916.1996.tb08608.x