Preparation of transparent mullite-silica film by heat-treatment of imogolite
Natural gel-like imogolite was dispersed in an acetic acid aqueous solution. An imogolite film was prepared by evaporating the solvent from the imogolite solution and then subjecting it to heat-treatment. It transformed to an amorphous film at around 500 C and then to a mullite-silica composite film...
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Veröffentlicht in: | Journal of materials science 1992-01, Vol.27 (22), p.6193-6196 |
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Hauptverfasser: | , , , |
Format: | Artikel |
Sprache: | eng |
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Online-Zugang: | Volltext |
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Zusammenfassung: | Natural gel-like imogolite was dispersed in an acetic acid aqueous solution. An imogolite film was prepared by evaporating the solvent from the imogolite solution and then subjecting it to heat-treatment. It transformed to an amorphous film at around 500 C and then to a mullite-silica composite film at around 1000 C without showing pores and cracks. The film heat treated to 1200 C showed high transparency as well as a low thermal expansion coefficient of about 4 x 10 exp(-6). 10 refs. |
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ISSN: | 0022-2461 1573-4803 |
DOI: | 10.1007/BF01133770 |