Formation of beta prime -SiAlON from a montmorillonite-polyacrylonitrile composite by carbothermal reduction: an NMR, TGA, XRD, and EM study

The products of carbothermal reduction in N sub 2 of a nanocomposite between dodecyl-ammonium-exchanged montmorillonite and polyacrylonitrile were studied. The only crystalline phase detected at 1000- 1300 degrees C was beta prime -SiAlON, having a much higher Si:Al ratio (7.05:1) than that of the p...

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Veröffentlicht in:Journal of materials science 1991-03, Vol.26 (6), p.1443-1453
Hauptverfasser: Bastow, T, Hardin, S G, Turney, T W
Format: Artikel
Sprache:eng
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Zusammenfassung:The products of carbothermal reduction in N sub 2 of a nanocomposite between dodecyl-ammonium-exchanged montmorillonite and polyacrylonitrile were studied. The only crystalline phase detected at 1000- 1300 degrees C was beta prime -SiAlON, having a much higher Si:Al ratio (7.05:1) than that of the precursor clay (2.44:1). 53 refs.
ISSN:0022-2461