Accurate mass screening of pesticide residues in wine by modified QuEChERS and LC-hybrid LTQ/Orbitrap-MS

Accurate mass screening of pesticide residues in wine by modified QuEChERS and LC-hybrid LTQ/Orbitrap-MS

•Method development, validation for multiclass pesticide determination in white/red wine.•QuEChERS extraction combined with UPLC-Orbitrap-MS was applied for the first time.•High performance of the method fulfilling validation requirements.•Expanded uncertainties were

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Veröffentlicht in:Food chemistry 2021-10, Vol.360, p.130008-130008, Article 130008
Hauptverfasser: Kosma, Christina I., Koloka, Ourania L., Albanis, Triantafyllos A., Konstantinou, Ioannis K.
Format: Artikel
Sprache:eng
Schlagworte:
Analytical methodology
Liquid chromatography–LTQ Orbitrap mass spectrometry
Pesticides
QuEChERS
Uncertainty
Wine
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Beschreibung
Zusammenfassung:•Method development, validation for multiclass pesticide determination in white/red wine.•QuEChERS extraction combined with UPLC-Orbitrap-MS was applied for the first time.•High performance of the method fulfilling validation requirements.•Expanded uncertainties were
ISSN:0308-8146
1873-7072
DOI:10.1016/j.foodchem.2021.130008