FTIR and Raman spectral study of the preparation of lead zirconate (PbZrO3) by a solgel process in a non-flowing air atmosphere

FTIR and Raman spectral study of the preparation of lead zirconate (PbZrO3) by a solgel process in a non-flowing air atmosphere

Lead zirconate (PZ) materials were prepared by a sol-gel process in a non-flowing air atmosphere with no continuous agitation using lead acetate and zirconium propoxide in methoxyethanol as the precursor materials. Fourier transform infrared and Raman spectroscopy were used to characterize the struc...

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Veröffentlicht in:Journal of materials science 1989, Vol.24 (11), p.3873-3877
Hauptverfasser: Li, Shu, Condrate, R. A., Jang, S. D., Spriggs, R. M.
Format: Artikel
Sprache:eng
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Zusammenfassung:Lead zirconate (PZ) materials were prepared by a sol-gel process in a non-flowing air atmosphere with no continuous agitation using lead acetate and zirconium propoxide in methoxyethanol as the precursor materials. Fourier transform infrared and Raman spectroscopy were used to characterize the structural changes that occurred during various stages of this preparation.
ISSN:0022-2461
1573-4803
DOI:10.1007/BF01168949