Electroreductive Coupling of Phthalic Anhydrides with α,β-Unsaturated Carbonyl Compounds: Synthesis of 1,4-Dihydroxynaphthalenes

Electroreductive Coupling of Phthalic Anhydrides with α,β-Unsaturated Carbonyl Compounds: Synthesis of 1,4-Dihydroxynaphthalenes

Electroreductive coupling of phthalic anhydrides with α,β-unsaturated carbonyl compounds in the presence of TMSCl and subsequent treatment with 1 M HCl gave 1,4-dihydroxynaphthalenes and 2-methyl-2,3-dihydronaphthalene-1,4-diones.

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Veröffentlicht in:Journal of organic chemistry 2020-11, Vol.85 (21), p.13973-13982
Hauptverfasser: Kise, Naoki, Yamamoto, Shota, Sakurai, Toshihiko
Format: Artikel
Sprache:eng
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Zusammenfassung:Electroreductive coupling of phthalic anhydrides with α,β-unsaturated carbonyl compounds in the presence of TMSCl and subsequent treatment with 1 M HCl gave 1,4-dihydroxynaphthalenes and 2-methyl-2,3-dihydronaphthalene-1,4-diones.
ISSN:0022-3263
1520-6904
DOI:10.1021/acs.joc.0c02000