Determination of 60 pesticides in hen eggs using the QuEChERS procedure followed by LC-MS/MS and GC-MS/MS

•A technique was developed for determining 60 multi-residue pesticides in eggs.•The quick, easy, cheap, effective, rugged, safe sample-preparation method was used.•Gas and liquid chromatographies were used to determine pesticide levels.•Validation data reveal good linearities, recoveries, specificit...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Food chemistry 2019-11, Vol.298, p.125050-125050, Article 125050
Hauptverfasser: Song, Nho-Eul, Lee, Jun Young, Mansur, Ahmad Rois, Jang, Hae Won, Lim, Min-Cheol, Lee, Yunyeol, Yoo, Miyoung, Nam, Tae Gyu
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:•A technique was developed for determining 60 multi-residue pesticides in eggs.•The quick, easy, cheap, effective, rugged, safe sample-preparation method was used.•Gas and liquid chromatographies were used to determine pesticide levels.•Validation data reveal good linearities, recoveries, specificities, and precisions.•The method can be used to routinely monitor pesticide residues in egg samples. An analytical method involving QuEChERS (quick, easy, cheap, effective, rugged, and safe) sample preparation, followed by LC-MS/MS and GC-MS/MS was developed and validated for the determination of 60 pesticides in eggs. Recoveries of 70–120% were achieved for selected pesticides and relative standard deviations
ISSN:0308-8146
1873-7072
DOI:10.1016/j.foodchem.2019.125050