Mechanochemical synthesis of N-doped porous carbon at room temperature

We report the one-pot mechanochemical synthesis of N-doped porous carbons at room temperature using a planetary ball mill. The fast reaction (5 minutes) between calcium carbide and cyanuric chloride proceeds in absence of any solvent and displays a facile bottom-up strategy that completely avoids ty...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Nanoscale 2019-03, Vol.11 (11), p.4712-4718
Hauptverfasser: Casco, Mirian Elizabeth, Kirchhoff, Sebastian, Leistenschneider, Desirée, Rauche, Marcus, Brunner, Eike, Borchardt, Lars
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:We report the one-pot mechanochemical synthesis of N-doped porous carbons at room temperature using a planetary ball mill. The fast reaction (5 minutes) between calcium carbide and cyanuric chloride proceeds in absence of any solvent and displays a facile bottom-up strategy that completely avoids typical thermal carbonization steps and directly yields a N-doped porous carbon containing 16 wt% of nitrogen and exhibiting a surface area of 1080 m2 g-1.
ISSN:2040-3364
2040-3372
DOI:10.1039/c9nr01019j