Recent Advances in High-Resolution Solid-State NMR Spectroscopy

Diverse complex systems may be studied by the new methods in solid‐state NMR spectroscopy described herein. These methods use magic‐angle spinning (MAS) on samples in oriented bilayers (right picture) and in orientationally disordered samples (left picture). Systems as diverse as uniformly 13C,15N‐labeled proteins, model membrane systems, and silk, as produced by the silkworm, can be structurally characterized.