Synthesis of 2‐d‐acrylamide
2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment. 2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxi...
Gespeichert in:
| Veröffentlicht in: | Journal of labelled compounds & radiopharmaceuticals 2018-06, Vol.61 (8), p.595-598 |
|---|---|
| Hauptverfasser: | , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 598 |
|---|---|
| container_issue | 8 |
| container_start_page | 595 |
| container_title | Journal of labelled compounds & radiopharmaceuticals |
| container_volume | 61 |
| creator | Salin, Alexey V. Musin, Rashid Z. |
| description | 2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment.
2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment. |
| doi_str_mv | 10.1002/jlcr.3603 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1989565904</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2059132886</sourcerecordid><originalsourceid>FETCH-LOGICAL-c3533-d95451fa5857c98e1161345012e94c88dfad2cd49956eecc7bf7c6528a8ab1613</originalsourceid><addsrcrecordid>eNp10MtKAzEUBuAgiq3VhS-gBTe6mDbXabIsg1cKgpd1SJMzOGWmU5MOMjsfwWf0SczY6kJwccjifPk5_AgdEzwiGNPxorR-xFLMdlCfYKUSwjjfRX3MUppwiVkPHYSwwDjuON9HPaoYZZzIPjp9bJfrFwhFGNb5kH6-f7g4xvq2NFXh4BDt5aYMcLR9B-j56vIpu0lm99e32XSWWCYYS5wSXJDcCCkmVkkgJI03CEwoKG6ldLlx1DqulEgBrJ3M84lNBZVGmnlnB-h8k7vy9WsDYa2rIlgoS7OEugmaKBm_CoV5pGd_6KJu_DJepykWijAqZRrVxUZZX4fgIdcrX1TGt5pg3bWmu9Z011q0J9vEZl6B-5U_NUUw3oC3ooT2_yR9N8seviO_AA2-dXw</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2059132886</pqid></control><display><type>article</type><title>Synthesis of 2‐d‐acrylamide</title><source>Wiley Online Library Journals Frontfile Complete</source><creator>Salin, Alexey V. ; Musin, Rashid Z.</creator><creatorcontrib>Salin, Alexey V. ; Musin, Rashid Z.</creatorcontrib><description>2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment.
2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment.</description><identifier>ISSN: 0362-4803</identifier><identifier>EISSN: 1099-1344</identifier><identifier>DOI: 10.1002/jlcr.3603</identifier><identifier>PMID: 29323418</identifier><language>eng</language><publisher>England: Wiley Subscription Services, Inc</publisher><subject>Acrylamide ; Acrylonitrile ; Deuterium ; deuterium‐labeled acrylamide ; deuterium‐labeled acrylonitrile ; electron‐deficient alkenes ; Heavy water ; hydration ; Isotopes ; Isotopic enrichment ; Organic chemistry</subject><ispartof>Journal of labelled compounds & radiopharmaceuticals, 2018-06, Vol.61 (8), p.595-598</ispartof><rights>Copyright © 2018 John Wiley & Sons, Ltd.</rights><rights>2018 John Wiley & Sons, Ltd.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3533-d95451fa5857c98e1161345012e94c88dfad2cd49956eecc7bf7c6528a8ab1613</citedby><cites>FETCH-LOGICAL-c3533-d95451fa5857c98e1161345012e94c88dfad2cd49956eecc7bf7c6528a8ab1613</cites><orcidid>0000-0002-2751-1666</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fjlcr.3603$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fjlcr.3603$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,27901,27902,45550,45551</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/29323418$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Salin, Alexey V.</creatorcontrib><creatorcontrib>Musin, Rashid Z.</creatorcontrib><title>Synthesis of 2‐d‐acrylamide</title><title>Journal of labelled compounds & radiopharmaceuticals</title><addtitle>J Labelled Comp Radiopharm</addtitle><description>2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment.
2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment.</description><subject>Acrylamide</subject><subject>Acrylonitrile</subject><subject>Deuterium</subject><subject>deuterium‐labeled acrylamide</subject><subject>deuterium‐labeled acrylonitrile</subject><subject>electron‐deficient alkenes</subject><subject>Heavy water</subject><subject>hydration</subject><subject>Isotopes</subject><subject>Isotopic enrichment</subject><subject>Organic chemistry</subject><issn>0362-4803</issn><issn>1099-1344</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNp10MtKAzEUBuAgiq3VhS-gBTe6mDbXabIsg1cKgpd1SJMzOGWmU5MOMjsfwWf0SczY6kJwccjifPk5_AgdEzwiGNPxorR-xFLMdlCfYKUSwjjfRX3MUppwiVkPHYSwwDjuON9HPaoYZZzIPjp9bJfrFwhFGNb5kH6-f7g4xvq2NFXh4BDt5aYMcLR9B-j56vIpu0lm99e32XSWWCYYS5wSXJDcCCkmVkkgJI03CEwoKG6ldLlx1DqulEgBrJ3M84lNBZVGmnlnB-h8k7vy9WsDYa2rIlgoS7OEugmaKBm_CoV5pGd_6KJu_DJepykWijAqZRrVxUZZX4fgIdcrX1TGt5pg3bWmu9Z011q0J9vEZl6B-5U_NUUw3oC3ooT2_yR9N8seviO_AA2-dXw</recordid><startdate>20180630</startdate><enddate>20180630</enddate><creator>Salin, Alexey V.</creator><creator>Musin, Rashid Z.</creator><general>Wiley Subscription Services, Inc</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><orcidid>https://orcid.org/0000-0002-2751-1666</orcidid></search><sort><creationdate>20180630</creationdate><title>Synthesis of 2‐d‐acrylamide</title><author>Salin, Alexey V. ; Musin, Rashid Z.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3533-d95451fa5857c98e1161345012e94c88dfad2cd49956eecc7bf7c6528a8ab1613</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Acrylamide</topic><topic>Acrylonitrile</topic><topic>Deuterium</topic><topic>deuterium‐labeled acrylamide</topic><topic>deuterium‐labeled acrylonitrile</topic><topic>electron‐deficient alkenes</topic><topic>Heavy water</topic><topic>hydration</topic><topic>Isotopes</topic><topic>Isotopic enrichment</topic><topic>Organic chemistry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Salin, Alexey V.</creatorcontrib><creatorcontrib>Musin, Rashid Z.</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of labelled compounds & radiopharmaceuticals</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Salin, Alexey V.</au><au>Musin, Rashid Z.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of 2‐d‐acrylamide</atitle><jtitle>Journal of labelled compounds & radiopharmaceuticals</jtitle><addtitle>J Labelled Comp Radiopharm</addtitle><date>2018-06-30</date><risdate>2018</risdate><volume>61</volume><issue>8</issue><spage>595</spage><epage>598</epage><pages>595-598</pages><issn>0362-4803</issn><eissn>1099-1344</eissn><abstract>2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment.
2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment.</abstract><cop>England</cop><pub>Wiley Subscription Services, Inc</pub><pmid>29323418</pmid><doi>10.1002/jlcr.3603</doi><tpages>4</tpages><orcidid>https://orcid.org/0000-0002-2751-1666</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0362-4803 |
| ispartof | Journal of labelled compounds & radiopharmaceuticals, 2018-06, Vol.61 (8), p.595-598 |
| issn | 0362-4803 1099-1344 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1989565904 |
| source | Wiley Online Library Journals Frontfile Complete |
| subjects | Acrylamide Acrylonitrile Deuterium deuterium‐labeled acrylamide deuterium‐labeled acrylonitrile electron‐deficient alkenes Heavy water hydration Isotopes Isotopic enrichment Organic chemistry |
| title | Synthesis of 2‐d‐acrylamide |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-03T13%3A39%3A29IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Synthesis%20of%202%E2%80%90d%E2%80%90acrylamide&rft.jtitle=Journal%20of%20labelled%20compounds%20&%20radiopharmaceuticals&rft.au=Salin,%20Alexey%20V.&rft.date=2018-06-30&rft.volume=61&rft.issue=8&rft.spage=595&rft.epage=598&rft.pages=595-598&rft.issn=0362-4803&rft.eissn=1099-1344&rft_id=info:doi/10.1002/jlcr.3603&rft_dat=%3Cproquest_cross%3E2059132886%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2059132886&rft_id=info:pmid/29323418&rfr_iscdi=true |