Synthesis of 2‐d‐acrylamide

2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment. 2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxi...

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Veröffentlicht in:	Journal of labelled compounds & radiopharmaceuticals 2018-06, Vol.61 (8), p.595-598
Hauptverfasser:	Salin, Alexey V., Musin, Rashid Z.
Format:	Artikel
Sprache:	eng
Schlagworte:	Acrylamide Acrylonitrile Deuterium deuterium‐labeled acrylamide deuterium‐labeled acrylonitrile electron‐deficient alkenes Heavy water hydration Isotopes Isotopic enrichment Organic chemistry
Online-Zugang:	Volltext
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Beschreibung
Zusammenfassung:	2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment. 2‐d‐Acrylamide was synthesized via the 2‐step procedure starting from acrylonitrile and deuterium oxide. This procedure affords 2‐d‐acrylamide in 99.9% chemical purity and 98.4% isotopic enrichment.
ISSN:	0362-4803 1099-1344
DOI:	10.1002/jlcr.3603