Development of an enantioseparation method for novel psychoactive drugs by HPLC using a Lux® Cellulose-2 column in polar organic phase mode

Highlights • New chiral HPLC separation method applicable for a broad spectrum of NPDs. • A Lux® Cellulose-2 column was used in polar organic phase mode. • 40 psychoactive compounds were separated into their enantiomers, successfully. • Analysis of real life samples seized by Austrian police. • All...

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Veröffentlicht in:	Forensic science international 2017-01, Vol.270, p.232-240
Hauptverfasser:	Taschwer, Magdalena, Grascher, Jörg, Schmid, Martin G
Format:	Artikel
Sprache:	eng
Schlagworte:	Amphetamines Capillary electrophoresis Cellulose Chlorinated polysaccharide-based stationary phase Chromatography Drugs Enantioseparation Experiments Forensic sciences HPLC Ions Methods Novel psychoactive drugs (NPDs) Pathology Psychotropic drugs
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Beschreibung
Zusammenfassung:	Highlights • New chiral HPLC separation method applicable for a broad spectrum of NPDs. • A Lux® Cellulose-2 column was used in polar organic phase mode. • 40 psychoactive compounds were separated into their enantiomers, successfully. • Analysis of real life samples seized by Austrian police. • All tested compounds are traded as racemic mixtures.
ISSN:	0379-0738 1872-6283
DOI:	10.1016/j.forsciint.2016.10.011