Synthesis of lanthanum aluminate by reverse chemical precipitation using pseudoboehmite as alumina precursor
Lanthanum aluminate was synthesized by using reverse precipitation. A lanthanum nitrate salt in solution allowed the precipitation of lanthanum hydroxide onto the surface of the pseudoboehmite particles. Pseudoboehmite was previously synthesized out of aluminum sulfate which after characterization p...
Gespeichert in:
Veröffentlicht in: | Applied radiation and isotopes 2016-11, Vol.117, p.96-99 |
---|---|
Hauptverfasser: | , , , |
Format: | Artikel |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | Lanthanum aluminate was synthesized by using reverse precipitation. A lanthanum nitrate salt in solution allowed the precipitation of lanthanum hydroxide onto the surface of the pseudoboehmite particles. Pseudoboehmite was previously synthesized out of aluminum sulfate which after characterization presents a poor crystallized structure. A Perovskite-type lanthanum aluminate was obtained at different temperature and calcination time. When calcination was set up to 1500°C to 3°C/min pure, high crystallinity and highly agglomerated lanthanum aluminate is obtained, relative density of 94% was reached.
•Lanthanum aluminate was synthesized by reverse precipitation out of pseudoboehmite.•Pseudoboehmite proved to be an advantageous lanthanum aluminate synthesis precursor.•A mechanism of formation of lanthanum aluminate is proposed. |
---|---|
ISSN: | 0969-8043 1872-9800 |
DOI: | 10.1016/j.apradiso.2016.01.026 |